Phenylmethyl 4,6-bis-O-(3-hydroxypropyl)-2,3-bis-O-(phenylmethyl)-alpha-D-glucopyranoside

Base Information

Chemical Name:Phenylmethyl 4,6-bis-O-(3-hydroxypropyl)-2,3-bis-O-(phenylmethyl)-alpha-D-glucopyranoside
CAS No.:245527-13-3
Molecular Formula:C33H42O8
Molecular Weight:0
Hs Code.:
Mol file:245527-13-3.mol

Synonyms:Phenylmethyl 4,6-bis-O-(3-hydroxypropyl)-2,3-bis-O-(phenylmethyl)-alpha-D-glucopyranoside

Suppliers and Price of Phenylmethyl 4,6-bis-O-(3-hydroxypropyl)-2,3-bis-O-(phenylmethyl)-alpha-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phenylmethyl 4,6-bis-O-(3-hydroxypropyl)-2,3-bis-O-(phenylmethyl)-alpha-D-glucopyranoside

Chemical Property:

Purity/Quality:

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Technology Process of Phenylmethyl 4,6-bis-O-(3-hydroxypropyl)-2,3-bis-O-(phenylmethyl)-alpha-D-glucopyranoside

There total 2 articles about Phenylmethyl 4,6-bis-O-(3-hydroxypropyl)-2,3-bis-O-(phenylmethyl)-alpha-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: Benzyl 2,3-di-O-benzyl-4,6-di-O-[3-(tetrahydro-2H-pyranyl)oxypropyl]-α-D-glucopyranoside

: 245527-13-3
Benzyl 2,3-di-O-benzyl-4,6-di-O-(3-hydroxypropyl)-α-D-glucopyranoside

Guidance literature:: With pyridinium p-toluenesulfonate; In methanol; at 60 ℃; for 3h;
DOI:10.1055/s-1999-3566

Reference yield:

: 58527-86-9
Benzyl 2,3-di-O-benzyl-α-D-glucopyranoside

: 245527-13-3
Benzyl 2,3-di-O-benzyl-4,6-di-O-(3-hydroxypropyl)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / NaH / dimethylformamide / 12 h / 20 °C

2: 75 percent / pyridinium p-toluenesulfonate / methanol / 3 h / 60 °C

With pyridinium p-toluenesulfonate; sodium hydride; In methanol; N,N-dimethyl-formamide; 1: Etherification / 2: dealkylation;
DOI:10.1055/s-1999-3566

Reference yield:

: 245527-13-3
Benzyl 2,3-di-O-benzyl-4,6-di-O-(3-hydroxypropyl)-α-D-glucopyranoside

: C₄₅H₄₈O₁₂P₂

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / toluene / 0 - 20 °C

2: 100 percent / CH₂Cl₂ / 1 h / 20 °C

In dichloromethane; toluene;
DOI:10.1515/znb-2000-1011