3-Methylperbenzoic acid tert-butyl ester

Base Information

• Chemical Name: 3-Methylperbenzoic acid tert-butyl ester
• CAS No.: 22313-61-7
• Molecular Formula: C₁₂H₁₆O₃
• Molecular Weight: 208.257
• Mol file: 22313-61-7.mol

Synonyms:3-Methylperbenzoic acid tert-butyl ester;m-Methylperbenzoic acid tert-butyl ester

Chemical Property of 3-Methylperbenzoic acid tert-butyl ester

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-Methylperbenzoic acid tert-butyl ester

There total 3 articles about 3-Methylperbenzoic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

tert.-butylhydroperoxide (75-91-2) + 3-Methylbenzoyl chloride (1711-06-4) → tert-butyl peroxy-m-methylbenzoate (22313-61-7)

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 0 ℃;

DOI:10.1016/S0040-4020(97)00322-0

Reference yield: 70.0%

tert.-butylhydroperoxide (75-91-2) + m-xylene (108-38-3,104809-90-7) → tert-butyl peroxy-m-methylbenzoate (22313-61-7)

Guidance literature:

With potassium iodide; In water; at 40 ℃; for 0.0166667h; Flow reactor; Green chemistry;

DOI:10.1021/acs.oprd.7b00248

Reference yield: 67.0%

tert.-butylhydroperoxide (75-91-2) + m-tolyl aldehyde (620-23-5) → tert-butyl peroxy-m-methylbenzoate (22313-61-7)

Guidance literature:

With tetra-(n-butyl)ammonium iodide; In water; at 40 ℃; for 24h;

DOI:10.1039/c1cc14602e

upstream raw materials:

tert.-butylhydroperoxide

3-Methylbenzoyl chloride

m-tolyl aldehyde

m-xylene

Downstream raw materials:

7-methyl-3,4-diphenyl-1H-2-benzopyran-1-one

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