1H-Indole-4-carboxylic acid,6-broMo-1-(1-Methylpropyl)-,Methyl ester

Base Information

Chemical Name:1H-Indole-4-carboxylic acid,6-broMo-1-(1-Methylpropyl)-,Methyl ester
CAS No.:1346576-37-1
Molecular Formula:C14H16BrNO2
Molecular Weight:310.18634
Hs Code.:
Mol file:1346576-37-1.mol

Synonyms:1H-Indole-4-carboxylic acid,6-broMo-1-(1-Methylpropyl)-,Methyl ester

Suppliers and Price of 1H-Indole-4-carboxylic acid,6-broMo-1-(1-Methylpropyl)-,Methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
Methyl6-bromo-1-(sec-butyl)-1H-indole-4-carboxylate 97%
5g
$ 982.00

Crysdot
Methyl6-bromo-1-(sec-butyl)-1H-indole-4-carboxylate 97%
1g
$ 327.00

ChemScene
1H-Indole-4-carboxylicacid,6-bromo-1-(1-methylpropyl)-,methylester >97.0%
250mg
$ 490.00

ChemScene
1H-Indole-4-carboxylicacid,6-bromo-1-(1-methylpropyl)-,methylester >97.0%
100mg
$ 295.00

ChemScene
1H-Indole-4-carboxylicacid,6-bromo-1-(1-methylpropyl)-,methylester >97.0%
1g
$ 980.00

Chemenu
Methyl6-bromo-1-(sec-butyl)-1H-indole-4-carboxylate 95%+
5g
$ 926.00

Chemenu
Methyl6-bromo-1-(sec-butyl)-1H-indole-4-carboxylate 95%+
1g
$ 309.00

Total 6 raw suppliers

Chemical Property of 1H-Indole-4-carboxylic acid,6-broMo-1-(1-Methylpropyl)-,Methyl ester

Chemical Property:

PSA：31.23000
LogP:4.16140

Purity/Quality:

NLT 98% ^*data from raw suppliers

Methyl6-bromo-1-(sec-butyl)-1H-indole-4-carboxylate 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1H-Indole-4-carboxylic acid,6-broMo-1-(1-Methylpropyl)-,Methyl ester

There total 5 articles about 1H-Indole-4-carboxylic acid,6-broMo-1-(1-Methylpropyl)-,Methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 78-76-2,5787-31-5
s-butyl bromide

: 107650-22-6
methyl 6-bromo-1-isopropyl-3-methyl-1H-indole-4-carboxylate

: 1346576-37-1
methyl 6-bromo-1-(sec-butyl)-1H-indole-4-carboxylate

Guidance literature:: methyl 6-bromo-1-isopropyl-3-methyl-1H-indole-4-carboxylate; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.333333h;

s-butyl bromide; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 16h;

Reference yield: 14.0%

: 1346576-37-1
methyl 6-bromo-1-(sec-butyl)-1H-indole-4-carboxylate

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 0.166667h;

In N,N-dimethyl-formamide; mineral oil; at 65 ℃; for 6h;

Reference yield:

: 107650-20-4
5-bromo-2-methyl-3-nitro-benzoic acid

: 1346576-37-1
methyl 6-bromo-1-(sec-butyl)-1H-indole-4-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium carbonate / N,N-dimethyl-formamide / 12 h / 60 °C

2.1: N,N-dimethyl-formamide / 12 h / 100 °C

2.2: 4 h / 80 °C

3.1: sodium hydride / N,N-dimethyl-formamide / 0.33 h / 0 °C

3.2: 16 h / 0 - 20 °C

With sodium hydride; sodium carbonate; In N,N-dimethyl-formamide;