4-(4-chlorophenyl)-1-methyl-1H-1,2,3-Triazole-5-carboxylic acid

Base Information

Chemical Name:4-(4-chlorophenyl)-1-methyl-1H-1,2,3-Triazole-5-carboxylic acid
CAS No.:1402465-84-2
Molecular Formula:C₁₀H₈ClN₃O₂
Molecular Weight:237.645
Hs Code.:
Mol file:1402465-84-2.mol

Synonyms:4-(4-chlorophenyl)-1-methyl-1H-1,2,3-Triazole-5-carboxylic acid

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Chemical Property of 4-(4-chlorophenyl)-1-methyl-1H-1,2,3-Triazole-5-carboxylic acid

Chemical Property:

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Technology Process of 4-(4-chlorophenyl)-1-methyl-1H-1,2,3-Triazole-5-carboxylic acid

There total 1 articles about 4-(4-chlorophenyl)-1-methyl-1H-1,2,3-Triazole-5-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1402465-83-1
4-(4-chlorophenyl)-1-methyl-1H-1,2,3-triazole-5-carbaldehyde

: 1402465-84-2
4-(4-chlorophenyl)-1-methyl-1H-1,2,3-triazole-5-carboxylic acid

Guidance literature:: With Oxone; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 1517-69-7
(R)-1-phenylethanol

: 1402465-84-2
4-(4-chlorophenyl)-1-methyl-1H-1,2,3-triazole-5-carboxylic acid

: 1402465-85-3
(R)-1-phenylethyl 4-(4-chlorophenyl)-1-methyl-1H-1,2,3-triazol-5-ylcarbamate

Guidance literature:: With diphenyl phosphoryl azide; triethylamine; In toluene; at 80 ℃; for 3h; Molecular sieve 3 ?;

Reference yield:

: 1402465-84-2
4-(4-chlorophenyl)-1-methyl-1H-1,2,3-triazole-5-carboxylic acid

: 1396007-65-0
1-{4'-[1-methyl-5-((R)-1-phenyl-ethoxycarbonylamino)-1H-[1,2,3]triazol-4-yl]biphenyl-4-yl}cyclopropanecarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; diphenyl phosphoryl azide / toluene / 3 h / 80 °C / Molecular sieve 3 ?

2: potassium phosphate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane; water / 2 h / 100 °C / Microwave irradiation; Sealed vial; Inert atmosphere

With potassium phosphate; diphenyl phosphoryl azide; triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,4-dioxane; water; toluene;