(R)-1-phenylethyl 4-(4-chlorophenyl)-1-methyl-1H-1,2,3-triazol-5-ylcarbamate

Base Information

Chemical Name:(R)-1-phenylethyl 4-(4-chlorophenyl)-1-methyl-1H-1,2,3-triazol-5-ylcarbamate
CAS No.:1402465-85-3
Molecular Formula:C₁₈H₁₇ClN₄O₂
Molecular Weight:356.812
Hs Code.:

Synonyms:(R)-1-phenylethyl 4-(4-chlorophenyl)-1-methyl-1H-1,2,3-triazol-5-ylcarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-1-phenylethyl 4-(4-chlorophenyl)-1-methyl-1H-1,2,3-triazol-5-ylcarbamate

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Technology Process of (R)-1-phenylethyl 4-(4-chlorophenyl)-1-methyl-1H-1,2,3-triazol-5-ylcarbamate

There total 2 articles about (R)-1-phenylethyl 4-(4-chlorophenyl)-1-methyl-1H-1,2,3-triazol-5-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1517-69-7
(R)-1-phenylethanol

: 1402465-84-2
4-(4-chlorophenyl)-1-methyl-1H-1,2,3-triazole-5-carboxylic acid

: 1402465-85-3
(R)-1-phenylethyl 4-(4-chlorophenyl)-1-methyl-1H-1,2,3-triazol-5-ylcarbamate

Guidance literature:: With diphenyl phosphoryl azide; triethylamine; In toluene; at 80 ℃; for 3h; Molecular sieve 3 ?;

Reference yield:

: 1402465-83-1
4-(4-chlorophenyl)-1-methyl-1H-1,2,3-triazole-5-carbaldehyde

: 1402465-85-3
(R)-1-phenylethyl 4-(4-chlorophenyl)-1-methyl-1H-1,2,3-triazol-5-ylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: Oxone / N,N-dimethyl-formamide / 20 °C

2: triethylamine; diphenyl phosphoryl azide / toluene / 3 h / 80 °C / Molecular sieve 3 ?

With Oxone; diphenyl phosphoryl azide; triethylamine; In N,N-dimethyl-formamide; toluene;

Reference yield:

: 1159489-46-9
[4-(1'-carboxycyclopropyl)phenyl]boronic acid

: 1402465-85-3
(R)-1-phenylethyl 4-(4-chlorophenyl)-1-methyl-1H-1,2,3-triazol-5-ylcarbamate

: 1396007-65-0
1-{4'-[1-methyl-5-((R)-1-phenyl-ethoxycarbonylamino)-1H-[1,2,3]triazol-4-yl]biphenyl-4-yl}cyclopropanecarboxylic acid

Guidance literature:: With potassium phosphate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,4-dioxane; water; at 100 ℃; for 2h; Microwave irradiation; Sealed vial; Inert atmosphere;