1,4,6-Tri-O-acetyl-2,3-O-isopropylidene-a-D-mannopyranose

Base Information

• Chemical Name: 1,4,6-Tri-O-acetyl-2,3-O-isopropylidene-a-D-mannopyranose
• CAS No.: 68791-17-3
• Molecular Formula: C15H22O9
• Molecular Weight: 346.33
• Mol file: 68791-17-3.mol

Synonyms:1,4,6-Tri-O-acetyl-2,3-O-isopropylidene-a-D-mannopyranose

Chemical Property of 1,4,6-Tri-O-acetyl-2,3-O-isopropylidene-a-D-mannopyranose

Chemical Property:

• Boiling Point: 412.8±45.0 °C(Predicted)
• PSA: 106.59000
• Density: 1.28±0.1 g/cm3(Predicted)
• LogP: 0.28930

Purity/Quality:

98% min ^*data from raw suppliers

1,4,6-Tri-O-acetyl-2,3-O-isopropylidene-a-D-mannopyranose ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,4,6-Tri-O-acetyl-2,3-O-isopropylidene-a-D-mannopyranose

There total 1 articles about 1,4,6-Tri-O-acetyl-2,3-O-isopropylidene-a-D-mannopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 1,4,6-tri-O-acetyl-2,3-O-isopropylidene-α-D-mannopyranose (68791-17-3)

Guidance literature:

4,6-Diol 15, Acetanhydrid;

DOI:10.1016/S0008-6215(00)84126-9

Reference yield: 70.0%

1,4,6-tri-O-acetyl-2,3-O-isopropylidene-α-D-mannopyranose (68791-17-3) + p-methoxybenzyl chloride (824-94-2) → 4-methoxybenzyl 4,6-di-O-acetyl-2,3-O-isopropylidene-α-D-mannopyranoside (1039505-83-3)

Guidance literature:

1,4,6-tri-O-acetyl-2,3-O-isopropylidene-α-D-mannopyranose; With hydrazine hydrate; In N,N-dimethyl-formamide; at 20 ℃; for 1.5h;

With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃;

p-methoxybenzyl chloride; In N,N-dimethyl-formamide; at 20 ℃; for 1h; Further stages.;

DOI:10.1021/jo800478a

Reference yield: 66.0%

1,4,6-tri-O-acetyl-2,3-O-isopropylidene-α-D-mannopyranose (68791-17-3) + 1-iodo-2-phenylethyne (932-88-7) → C21H24O7 (1013036-26-4)

Guidance literature:

With indium; In dichloromethane; for 24h; stereoselective reaction; Reflux;

DOI:10.1021/ol7029257

Downstream raw materials:

4-methoxybenzyl 4,6-di-O-acetyl-2,3-O-isopropylidene-α-D-mannopyranoside

C₂₁H₂₄O₇

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