1,2-Cyclohexanediol di(methanesulfonate)

Base Information

• Chemical Name: 1,2-Cyclohexanediol di(methanesulfonate)
• CAS No.: 55724-11-3
• Molecular Formula: C8H16O6S2
• Molecular Weight: 272.343
• Mol file: 55724-11-3.mol

Synonyms:1,2-Cyclohexanediol di(methanesulfonate)

Chemical Property of 1,2-Cyclohexanediol di(methanesulfonate)

Chemical Property:

• PSA: 103.50000
• LogP: 2.41160

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,2-Cyclohexanediol di(methanesulfonate)

There total 5 articles about 1,2-Cyclohexanediol di(methanesulfonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

trans-1,2-cyclohexandiol (1460-57-7) + methanesulfonyl chloride (124-63-0) → trans-1,2-bis(methanesulphonyl)cyclohexane (38932-04-6,39967-15-2,55724-11-3)

Guidance literature:

With pyridine; at 0 ℃;

DOI:10.1016/S0040-4039(01)94068-7

Reference yield:

1,2-Cyclohexanediol (931-17-9) + methanesulfonyl chloride (124-63-0) → dimesylate of trans-1,2-cyclohexanediol (55724-11-3)

Guidance literature:

With triethylamine; Inert atmosphere;

DOI:10.1002/adsc.200900708

Reference yield:

trans-1,2-cyclohexandiol (1460-57-7) → trans-1,2-bis(methanesulphonyl)cyclohexane (38932-04-6,39967-15-2,55724-11-3)

Guidance literature:

DOI:10.1039/jr9490000315

upstream raw materials:

trans-1,2-cyclohexandiol

methanesulfonyl chloride

trans-2-acetoxy-1-cyclohexanol

1,2-Cyclohexanediol

Downstream raw materials:

trans-2-(mercaptomethyl)cyclohexanol

(+/-)-trans-2-methylcyclohexanol

trans-1,2-bis(phenylselenenyl)cyclohexane

Refernces