4-(2,5-DIMETHYL-PYRROL-1-YL)-PIPERIDINE

Base Information

• Chemical Name: 4-(2,5-DIMETHYL-PYRROL-1-YL)-PIPERIDINE
• CAS No.: 1032289-55-6
• Molecular Formula: C11H18N2
• Molecular Weight: 178.27
• Hs Code.: 2933990090
• Mol file: 1032289-55-6.mol

Synonyms:4-(2,5-DIMETHYL-PYRROL-1-YL)-PIPERIDINE;4-(2,5-Dimethyl-1H-pyrrol-1-yl)piperidine

Chemical Property of 4-(2,5-DIMETHYL-PYRROL-1-YL)-PIPERIDINE

Chemical Property:

• PSA: 16.96000
• LogP: 2.35820

Purity/Quality:

97% ^*data from raw suppliers

4-(2,5-Dimethyl-pyrrol-1-yl)-piperidine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-(2,5-DIMETHYL-PYRROL-1-YL)-PIPERIDINE

There total 6 articles about 4-(2,5-DIMETHYL-PYRROL-1-YL)-PIPERIDINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

tert-butyl 4-(2,5-dimethyl-1H-pyrrol-1-yl)piperidine-1-carboxylate → 4-(2,5-dimethyl-1H-pyrrol-1-yl)piperidine (1032289-55-6)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; at 0 ℃; for 3h;

DOI:10.1002/cmdc.201300177

Reference yield:

4-amino-1-benzylpiperidine (50541-93-0) + 2,5-hexanedione (110-13-4) → 4-(2,5-dimethyl-1H-pyrrol-1-yl)piperidine (1032289-55-6)

Guidance literature:

4-amino-1-benzylpiperidine; 2,5-hexanedione; With acetic acid; In toluene; for 4h; Heating;

With hydrogen; palladium dihydroxide; In methanol; at 20 ℃; for 24h; under 3040.2 Torr; Further stages.;

DOI:10.1080/00397910701845795

Reference yield:

1-benzyl-4-(2,5-dimethyl-1H-pyrrol-1-yl)piperidine (1108147-59-6) → 4-(2,5-dimethyl-1H-pyrrol-1-yl)piperidine (1032289-55-6)

Guidance literature:

With hydrogen; palladium(II) hydroxide; In methanol; at 20 ℃; for 16h;

DOI:10.1021/jm7012979

upstream raw materials:

4-amino-1-benzylpiperidine

2,5-hexanedione

1-benzyl-4-(2,5-dimethyl-1H-pyrrol-1-yl)piperidine

1-(tert-butoxycarbonyl)-4-aminopiperidine

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