Technology Process of Naphthalene, 2-iodo-7-methoxy- (9CI)
There total 4 articles about Naphthalene, 2-iodo-7-methoxy- (9CI) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
molecular sieve; Amberlyst XN-1010 resin; potassium iodide;
In
N,N-dimethyl-formamide; acetonitrile;
at 70 ℃;
DOI:10.1021/jo00312a036
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 46 percent / bucherer reaction
2: 97 percent / standard conditions
3: 1) aq. HCl, NaNO2, 2) K2CO3 / 1) H2O, 0 deg C, 1 h, 2) H2O
4: 33.1 percent / KI, Amberlyst XN-1010 resin, ground molecular sieve / acetonitrile; dimethylformamide / 70 °C
With
hydrogenchloride; molecular sieve; Amberlyst XN-1010 resin; potassium carbonate; potassium iodide; sodium nitrite;
In
N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo00312a036
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 97 percent / standard conditions
2: 1) aq. HCl, NaNO2, 2) K2CO3 / 1) H2O, 0 deg C, 1 h, 2) H2O
3: 33.1 percent / KI, Amberlyst XN-1010 resin, ground molecular sieve / acetonitrile; dimethylformamide / 70 °C
With
hydrogenchloride; molecular sieve; Amberlyst XN-1010 resin; potassium carbonate; potassium iodide; sodium nitrite;
In
N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo00312a036
