1-(4-ethoxycarbonylphenyl)-2-oxo-1,2-dihydropyridine-4-carboxylic acid, triethylammonium salt

Base Information

Chemical Name:1-(4-ethoxycarbonylphenyl)-2-oxo-1,2-dihydropyridine-4-carboxylic acid, triethylammonium salt
CAS No.:1256385-28-0
Molecular Formula:C₆H₁₅N*C₁₅H₁₃NO₅
Molecular Weight:388.464
Hs Code.:
Mol file:1256385-28-0.mol

Synonyms:1-(4-ethoxycarbonylphenyl)-2-oxo-1,2-dihydropyridine-4-carboxylic acid, triethylammonium salt

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Chemical Property of 1-(4-ethoxycarbonylphenyl)-2-oxo-1,2-dihydropyridine-4-carboxylic acid, triethylammonium salt

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Technology Process of 1-(4-ethoxycarbonylphenyl)-2-oxo-1,2-dihydropyridine-4-carboxylic acid, triethylammonium salt

There total 1 articles about 1-(4-ethoxycarbonylphenyl)-2-oxo-1,2-dihydropyridine-4-carboxylic acid, triethylammonium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 51934-41-9
4-iodobenzoic acid ethyl ester

: 89937-77-9
methyl 2-oxo-1,2-dihydropyridine-4-carboxylate

: 121-44-8
triethylamine

: 1256385-28-0
1-(4-ethoxycarbonylphenyl)-2-oxo-1,2-dihydropyridine-4-carboxylic acid, triethylammonium salt

Guidance literature:: methyl 2-oxo-1,2-dihydropyridine-4-carboxylate; With tetra(n-butyl)ammonium hydroxide; In water; toluene; at 20 ℃; for 2h;

4-iodobenzoic acid ethyl ester; With copper(l) iodide; In N,N-dimethyl-formamide; at 95 ℃; for 18h; Protection from light;

triethylamine; In methanol; dichloromethane;

Reference yield:

: 1256385-28-0
1-(4-ethoxycarbonylphenyl)-2-oxo-1,2-dihydropyridine-4-carboxylic acid, triethylammonium salt

: 1256385-29-1
1-(4-carboxyphenyl)-2-oxo-1,2-dihydropyridine-4-carboxylic acid

Guidance literature:: 1-(4-ethoxycarbonylphenyl)-2-oxo-1,2-dihydropyridine-4-carboxylic acid, triethylammonium salt; With water; sodium hydroxide; In tetrahydrofuran; at 0 - 20 ℃;

With hydrogenchloride; In tetrahydrofuran; water; pH=1;

Reference yield:

: 1256385-28-0
1-(4-ethoxycarbonylphenyl)-2-oxo-1,2-dihydropyridine-4-carboxylic acid, triethylammonium salt

: C₁₃H₇Cl₂NO₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: water; sodium hydroxide / tetrahydrofuran / 0 - 20 °C

1.2: pH 1

2.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 4 h / 20 °C

With oxalyl dichloride; water; sodium hydroxide; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane;