(S)-1-Methyl-3-aMinoMethy...

Base Information

• Chemical Name: (S)-1-Methyl-3-aMinoMethy...
• CAS No.: 1217604-20-0
• Molecular Formula: C₇H₁₆N₂
• Molecular Weight: 128.217
• Hs Code.: 2933399090
• Mol file: 1217604-20-0.mol

Synonyms:(S)-1-Methyl-3-aMinoMethy...;(S)-1-Methyl-3-aMinoMethyl-piperidine

Chemical Property of (S)-1-Methyl-3-aMinoMethy...

Chemical Property:

• Boiling Point: 155.3±8.0 °C(Predicted)
• PKA: 10.12±0.29(Predicted)
• PSA: 29.26000
• Density: 0.901±0.06 g/cm3(Predicted)
• LogP: 0.92510

Purity/Quality:

98%,99%, ^*data from raw suppliers

(S)-1-Methyl-3-aminomethyl-piperidine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (S)-1-Methyl-3-aMinoMethy...

There total 6 articles about (S)-1-Methyl-3-aMinoMethy... which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

3-(di-tert-butoxycarbonylaminomethyl)-1-methylpiperidine (672324-98-0) → [(3RS)-1-methyl-3-piperidyl] methylamine (14613-37-7,1217604-20-0)

Guidance literature:

With sulfuric acid; In 1,4-dioxane; methanol; at 25 ℃; for 0.5h;

Reference yield:

3-Aminomethylpyridine (3731-52-0) → [(3RS)-1-methyl-3-piperidyl] methylamine (14613-37-7,1217604-20-0)

Guidance literature:

Reference yield:

→ [(3RS)-1-methyl-3-piperidyl] methylamine (14613-37-7,1217604-20-0)

Guidance literature:

With lithium aluminium tetrahydride; diethyl ether;

upstream raw materials:

3-(di-tert-butoxycarbonylaminomethyl)-1-methylpiperidine

3-Aminomethylpyridine

Refernces

• 1、 -. "N-SUBSTITUTED-N'-SUBSTITUTED UREA DERIVATIVE AND USE THEREOF AS TNF-γ(a) PRODUCTION INHIBITOR". Page 9. . Retrieved 2008/06/13.