3-bromo-2-iodo-5-methylbenzoic acid

Base Information

• Chemical Name: 3-bromo-2-iodo-5-methylbenzoic acid
• CAS No.: 750585-99-0
• Molecular Formula: C8H6BrIO2
• Molecular Weight: 340.943
• Mol file: 750585-99-0.mol

Synonyms:3-bromo-2-iodo-5-methylbenzoic acid

Chemical Property of 3-bromo-2-iodo-5-methylbenzoic acid

Chemical Property:

• PSA: 37.30000
• LogP: 3.06030

Purity/Quality:

99% ^*data from raw suppliers

3-Bromo-2-iodo-5-methyl-benzoicacid 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-bromo-2-iodo-5-methylbenzoic acid

There total 1 articles about 3-bromo-2-iodo-5-methylbenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-amino-3-bromo-5-methylbenzoic acid (13091-43-5) → 3-bromo-2-iodo-5-methylbenzoic acid (750585-99-0)

Guidance literature:

2-amino-3-bromo-5-methylbenzoic acid; With sulfuric acid; sodium nitrite; In water; at 0 - 5 ℃; for 0.75h;

With potassium iodide; In water;

Reference yield:

3-bromo-2-iodo-5-methylbenzoic acid (750585-99-0) → 3-bromo-2-iodo-5-methylbenzamide

Guidance literature:

3-bromo-2-iodo-5-methylbenzoic acid; With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;

With ammonium hydroxide; In tetrahydrofuran; at 0 ℃; for 0.333333h; Inert atmosphere;

DOI:10.1002/anie.201914876

upstream raw materials:

2-amino-3-bromo-5-methylbenzoic acid