1-(3-But-3-enylphenyl)ethanone

Base Information

Chemical Name:1-(3-But-3-enylphenyl)ethanone
CAS No.:358751-04-9
Molecular Formula:C12H14O
Molecular Weight:174.243
Hs Code.:2914399090
DSSTox Substance ID:DTXSID40446761
Wikidata:Q82265482
Mol file:358751-04-9.mol

Synonyms:1-(3-but-3-enylphenyl)ethanone;358751-04-9;DTXSID40446761;AKOS006306415;1-[3-(but-3-en-1-yl)phenyl]ethan-1-one

Suppliers and Price of 1-(3-But-3-enylphenyl)ethanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 1-(3-But-3-enylphenyl)ethanone

Chemical Property:

PSA：17.07000
LogP:3.00780
XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:174.104465066
Heavy Atom Count:13
Complexity:184

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)C1=CC=CC(=C1)CCC=C

Technology Process of 1-(3-But-3-enylphenyl)ethanone

There total 4 articles about 1-(3-But-3-enylphenyl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 108-24-7
acetic anhydride

: 161173-98-4
1-bromo-3-(but-3-en-1-yl)benzene

: 358751-04-9
1-(3-but-3-enyl-phenyl)-ethanone

Guidance literature:: 1-bromo-3-(but-3-en-1-yl)benzene; With magnesium; In tetrahydrofuran;

acetic anhydride; In tetrahydrofuran; at -78 ℃; Further stages.;
DOI:10.1021/ja016642j

Reference yield:

: 823-78-9
meta-bromobenzyl bromide

: 358751-04-9
1-(3-but-3-enyl-phenyl)-ethanone

Guidance literature:: Multi-step reaction with 2 steps

1.1: 84 percent / diethyl ether; tetrahydrofuran / 2 h

2.1: magnesium / tetrahydrofuran

2.2: 67 percent / tetrahydrofuran / -78 °C

With magnesium; In tetrahydrofuran; diethyl ether;
DOI:10.1021/ja016642j