N-[1-[[(cyanomethyl)amino]carbonyl]cyclohexyl]-, 1,1-dimethylethyl ester

Base Information

Chemical Name:N-[1-[[(cyanomethyl)amino]carbonyl]cyclohexyl]-, 1,1-dimethylethyl ester
CAS No.:225122-33-8
Molecular Formula:C₁₄H₂₃N₃O₃
Molecular Weight:281.355
Hs Code.:
Mol file:225122-33-8.mol

Synonyms:N-[1-[[(cyanomethyl)amino]carbonyl]cyclohexyl]-, 1,1-dimethylethyl ester

Suppliers and Price of N-[1-[[(cyanomethyl)amino]carbonyl]cyclohexyl]-, 1,1-dimethylethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 2 raw suppliers

Chemical Property of N-[1-[[(cyanomethyl)amino]carbonyl]cyclohexyl]-, 1,1-dimethylethyl ester

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

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Hazard Codes:

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Technology Process of N-[1-[[(cyanomethyl)amino]carbonyl]cyclohexyl]-, 1,1-dimethylethyl ester

There total 4 articles about N-[1-[[(cyanomethyl)amino]carbonyl]cyclohexyl]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 6011-14-9
2-aminoacetonitrile hydrochloride

: 115951-16-1
1-tert-butoxycarbonylaminocyclohexanecarboxylic acid

: 225122-33-8
N-(tert-butyloxycarbonyl)homocycloleucyl-glycine-nitrile

Guidance literature:: With triethylamine; HATU; In N,N-dimethyl-formamide; Inert atmosphere;
DOI:10.1002/chem.201100113

Reference yield: 67.0%

: 151-63-3
cyanomethylamine sulfate

: 115951-16-1
1-tert-butoxycarbonylaminocyclohexanecarboxylic acid

: 225122-33-8
N-(tert-butyloxycarbonyl)homocycloleucyl-glycine-nitrile

Guidance literature:: 1-tert-butoxycarbonylaminocyclohexanecarboxylic acid; With triethylamine; isobutyl chloroformate; In tetrahydrofuran; at -25 ℃; for 0.0833333h;

cyanomethylamine sulfate; In tetrahydrofuran; at -25 - 20 ℃;
DOI:10.1002/chem.201101350

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 225122-33-8
N-(tert-butyloxycarbonyl)homocycloleucyl-glycine-nitrile

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / water; acetone / Inert atmosphere

2: triethylamine; HATU / N,N-dimethyl-formamide / Inert atmosphere

With triethylamine; HATU; sodium hydroxide; In water; N,N-dimethyl-formamide; acetone;
DOI:10.1002/chem.201100113