Technology Process of 1-Methyl-2,3-diphenylazetidine
There total 5 articles about 1-Methyl-2,3-diphenylazetidine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; 1,3-bis-(diphenylphosphino)propane; phenylsilane;
In
tetrahydrofuran;
at 50 ℃;
for 3h;
Inert atmosphere;
Schlenk technique;
DOI:10.1002/ejoc.201403655
- Guidance literature:
-
With
lithium aluminium tetrahydride; aluminium trichloride;
In
tetrahydrofuran; diethyl ether;
at 0 ℃;
for 45h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: copper(l) iodide; sodium acetate; potassium hydrogencarbonate; [2,2]bipyridinyl / 18 h / 70 °C / Inert atmosphere; Schlenk technique; Sealed tube
2: bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; 1,3-bis-(diphenylphosphino)propane; phenylsilane / tetrahydrofuran / 3 h / 50 °C / Inert atmosphere; Schlenk technique
With
[2,2]bipyridinyl; copper(l) iodide; bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; 1,3-bis-(diphenylphosphino)propane; phenylsilane; sodium acetate; potassium hydrogencarbonate;
In
tetrahydrofuran;
1: |Kinugasa B-Lactam Synthesis;
DOI:10.1002/ejoc.201403655
