2-chloro-6-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)aniline

Base Information

Chemical Name:2-chloro-6-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)aniline
CAS No.:1309982-17-9
Molecular Formula:C₁₂H₁₇BClNO₂
Molecular Weight:253.536
Hs Code.:2934999090
Mol file:1309982-17-9.mol

Synonyms:2-chloro-6-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)aniline;2-CHLORO-6-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)-BENZENAMINE

Suppliers and Price of 2-chloro-6-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)aniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
2-Chloro-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline 95+%
1g
$ 491.00

Alichem
2-Chloro-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline
1g
$ 400.00

Total 6 raw suppliers

Chemical Property of 2-chloro-6-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)aniline

Chemical Property:

PSA：44.48000
LogP:2.80260
Storage Temp.:2-8°C

Purity/Quality:

97% ^*data from raw suppliers

2-Chloro-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-chloro-6-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)aniline

There total 2 articles about 2-chloro-6-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 95-51-2
o-chloroaniline

: 1309982-17-9
2-chloro-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline

Guidance literature:: Multi-step reaction with 2 steps

1.1: (1,5-cyclooctadiene)(methoxy)iridium(I) dimer / tetrahydrofuran / 0.17 h / 80 °C

1.2: 12 h / 80 °C

2.1: chloroform / 1 h / 20 °C

With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; In tetrahydrofuran; chloroform;
DOI:10.1021/acscatal.8b00641

Reference yield:

: C₁₀H₁₂B₂ClNO₄

: 73183-34-3
bis(pinacol)diborane

: 1309982-17-9
2-chloro-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline

Guidance literature:: In chloroform; at 20 ℃; for 1h; regioselective reaction;
DOI:10.1021/acscatal.8b00641

Reference yield: 80.0%

: 1309982-17-9
2-chloro-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline

: C₃₆H₂₃BrClN

: C₄₂H₂₈Cl₂N₂

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In ethanol; water; toluene; at 110 ℃; Inert atmosphere;