Ethanone, 1-(4-Methyl-2-nitrophenyl)

Base Information

• Chemical Name: Ethanone, 1-(4-Methyl-2-nitrophenyl)
• CAS No.: 155694-84-1
• Molecular Formula: C9H9NO3
• Molecular Weight: 179.175
• Mol file: 155694-84-1.mol

Synonyms:Ethanone, 1-(4-Methyl-2-nitrophenyl);1-(4-methyl-2-nitrophenyl)ethanone

Chemical Property of Ethanone, 1-(4-Methyl-2-nitrophenyl)

Chemical Property:

• PSA: 62.89000
• LogP: 2.62900

Purity/Quality:

99% ^*data from raw suppliers

1-(4-Methyl-2-nitrophenyl)-ethanone ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Ethanone, 1-(4-Methyl-2-nitrophenyl)

There total 7 articles about Ethanone, 1-(4-Methyl-2-nitrophenyl) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

(E)-1-(4-methyl-2-nitrophenyl)ethanone O-methyl oxime (1439930-68-3) → 1-(4-methyl-2-nitrophenyl)ethan-1-one (155694-84-1)

Guidance literature:

With hydrogenchloride; water; In dichloromethane; at 100 ℃; for 24h; Sealed tube;

DOI:10.1021/jo400594j

Reference yield: 70.0%

4-methyl-2-nitro-1-(prop-1-en-2-yl)benzene (1449199-73-8) → 1-(4-methyl-2-nitrophenyl)ethan-1-one (155694-84-1)

Guidance literature:

4-methyl-2-nitro-1-(prop-1-en-2-yl)benzene; With ozone; In methanol; dichloromethane; at -78 ℃; for 3h;

With dimethylsulfide; In methanol; dichloromethane; at 20 ℃;

Reference yield:

C9H10N2O4 → 1-(4-methyl-2-nitrophenyl)ethan-1-one (155694-84-1)

Guidance literature:

With dihydrogen peroxide; sodium hydrogencarbonate; In methanol; water; at 20 ℃;

upstream raw materials:

3-(4-methyl-2-nitro-phenyl)-3-oxo-propionic acid

water

(E)-1-(4-methyl-2-nitrophenyl)ethanone O-methyl oxime

4-methyl-2-nitro-1-(prop-1-en-2-yl)benzene

Downstream raw materials:

2’-amino-4’-methylacetophenone

1-N-acetyl-4-keto-7-methyl-2-phenyl-3-(phenylseleno)-1,2,3,4-tetrahydroquinoline

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