2-Cyano-2-propyl 4-cyanobenzodithioate

Base Information

Chemical Name:2-Cyano-2-propyl 4-cyanobenzodithioate
CAS No.:851729-48-1
Molecular Formula:C12H10N2S2
Molecular Weight:246.357
Hs Code.:
Mol file:851729-48-1.mol

Synonyms:2-Cyano-2-propyl 4-cyanobenzodithioate ;2-Cyano-2-propyl 4-cyanobenzodithioate 98% (HPLC)

Suppliers and Price of 2-Cyano-2-propyl 4-cyanobenzodithioate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
2-Cyano-2-propyl 4-cyanobenzodithioate 98% (HPLC)
5g
$ 636.00

Sigma-Aldrich
2-Cyano-2-propyl 4-cyanobenzodithioate 98% (HPLC)
1g
$ 167.00

Total 3 raw suppliers

Chemical Property of 2-Cyano-2-propyl 4-cyanobenzodithioate

Chemical Property:

Melting Point:122-127°C
Boiling Point:407.0±55.0 °C(Predicted)
PSA：104.97000
Density:1.25±0.1 g/cm3(Predicted)
LogP:3.26916

Purity/Quality:

98%,99%, ^*data from raw suppliers

2-Cyano-2-propyl 4-cyanobenzodithioate 98% (HPLC) ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xi
Statements: 43
Safety Statements: 36/37

MSDS Files:: SDS file from LookChem

Useful:

Uses RAFT agent for controlled radical polymerization; especially suited for the polymerization of methyl methacrylate and styrene monomers. Chain Transfer Agent (CTA)

Technology Process of 2-Cyano-2-propyl 4-cyanobenzodithioate

There total 2 articles about 2-Cyano-2-propyl 4-cyanobenzodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 851729-35-6
bis(4-cyanothiobenzoyl) disulfide

: 78-67-1
2,2'-azobis(isobutyronitrile)

: 851729-48-1
2-cyanoprop-2-yl 4-cyanodithiobenzoate

Guidance literature:: In ethyl acetate; Heating;
DOI:10.1021/ma0480650

Reference yield:

: 17201-43-3
4-cyanobenzyl bromide

: 851729-48-1
2-cyanoprop-2-yl 4-cyanodithiobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaOMe; sulfur / methanol / 3 h

1.2: I₂ / H₂O

2.1: 35 percent / ethyl acetate / Heating

With sodium methylate; sulfur; In methanol; ethyl acetate;
DOI:10.1021/ma0480650