2-(4'-broMobiphenyl-4-yl)-4,4,5,5-tetraMethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:2-(4'-broMobiphenyl-4-yl)-4,4,5,5-tetraMethyl-1,3,2-dioxaborolane
CAS No.:1414997-84-4
Molecular Formula:C18H20BBrO2
Molecular Weight:359.0652
Hs Code.:
Mol file:1414997-84-4.mol

Synonyms:2-(4'-broMobiphenyl-4-yl)-4,4,5,5-tetraMethyl-1,3,2-dioxaborolane

Suppliers and Price of 2-(4'-broMobiphenyl-4-yl)-4,4,5,5-tetraMethyl-1,3,2-dioxaborolane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 3 raw suppliers

Chemical Property of 2-(4'-broMobiphenyl-4-yl)-4,4,5,5-tetraMethyl-1,3,2-dioxaborolane

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of 2-(4'-broMobiphenyl-4-yl)-4,4,5,5-tetraMethyl-1,3,2-dioxaborolane

There total 7 articles about 2-(4'-broMobiphenyl-4-yl)-4,4,5,5-tetraMethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 61676-62-8
2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 92-86-4
4-(4-bromophenyl)bromobenzene

: 1414997-84-4
2-(4'-bromo-[1,1'-biphenyl]-4-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: 4-(4-bromophenyl)bromobenzene; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃; for 1.52778E-05h;

2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane; In tetrahydrofuran; hexane; at 0 ℃; for 0.0025h;
DOI:10.1039/c2cc36197c

Reference yield: 56.0%

: 1186026-67-4
1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-4-(trimethylsilyl)benzene

: 673-40-5
4-bromobenzenediazonium tetrafluoroborate

: 1414997-84-4
2-(4'-bromo-[1,1'-biphenyl]-4-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With [bis(trifluoromethanesulfonyl)imidate](triphenylphosphine)gold(I); In acetonitrile; at -78 - 20 ℃; for 10h; chemoselective reaction; Inert atmosphere; Irradiation;
DOI:10.1002/anie.201806427

Reference yield:

: triethyl(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)germane

: 106-40-1
4-bromo-aniline

: 1414997-84-4
2-(4'-bromo-[1,1'-biphenyl]-4-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: 4-bromo-aniline; With tetrafluoroboric acid; isopentyl nitrite; In ethanol; water; at -20 - 20 ℃; for 1h; Inert atmosphere;

triethyl(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)germane; With (triphenylphosphine)gold(I) chloride; In acetonitrile; at 20 ℃; for 2h; Inert atmosphere; Irradiation; Glovebox;
DOI:10.1002/anie.202005066