Cyclopropanamine, 1-(4-chlorophenyl)-, hydrochloride (1:1)

Base Information

• Chemical Name: Cyclopropanamine, 1-(4-chlorophenyl)-, hydrochloride (1:1)
• CAS No.: 1009102-44-6
• Molecular Formula: C9H11Cl2N
• Molecular Weight: 204.099
• Hs Code.: 2921499090
• Mol file: 1009102-44-6.mol

Synonyms:Cyclopropanamine, 1-(4-chlorophenyl)-, hydrochloride (1:1);1-(4-Chlorophenyl)cyclopropanamine Hydrochloride

Chemical Property of Cyclopropanamine, 1-(4-chlorophenyl)-, hydrochloride (1:1)

Chemical Property:

• PSA: 26.02000
• LogP: 3.79010
• Storage Temp.: Inert atmosphere,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

1-(4-Chlorophenyl)cyclopropanamineHydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Cyclopropanamine, 1-(4-chlorophenyl)-, hydrochloride (1:1)

There total 1 articles about Cyclopropanamine, 1-(4-chlorophenyl)-, hydrochloride (1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.3%

4-Cyanochlorobenzene (623-03-0) + ethylmagnesium bromide (925-90-6) → 1-(4-chlorophenyl)cyclopropane-1-amine hydrochloride (1009102-44-6)

Guidance literature:

4-Cyanochlorobenzene; ethylmagnesium bromide; With titanium(IV) isopropylate; In tert-butyl methyl ether; at 0 - 20 ℃; for 1h;

With boron trifluoride diethyl etherate; In tert-butyl methyl ether; at 0 - 20 ℃; for 17h;

With hydrogenchloride; In ethyl acetate;

Reference yield: 100.0%

1-(4-chlorophenyl)cyclopropane-1-amine hydrochloride (1009102-44-6) + (E)-3-((3aS,5aR,5bR,7aR,9S,11aR,11bR,13aS)-9-hydroxy-1-isopropyl-5a,5b,8,8,11a-pentamethyl-2-oxo-3,3a,4,5,5a,5b,6,7,7a,8,9,10,11,11a,11b,12,13,13a-octadecahydro-2H-cyclopenta[a]chrysen-3a-yl)acrylic acid (1443513-36-7) → (E)-N-(1-(4-chlorophenyl)cyclopropyl)-3-((3aS,5aR,5bR,7aR,9S,11aR,11bR,13aS)-9-hydroxy-1-isopropyl-5a,5b,8,8,11a-pentamethyl-2-oxo-3,3a,4,5,5a,5b,6,7,7a,8,9,10,11,11a,11b,12,13,13a-octadecahydro-2H-cyclopenta[a]chrysen-3a-yl)acrylamide (1443513-37-8)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 1h;

Reference yield: 99.0%

1-(4-chlorophenyl)cyclopropane-1-amine hydrochloride (1009102-44-6) + (E)-3-((3aS,5aR,5bR,7aR,9S,11aR,11bR,13aS)-9-hydroxy-1-isopropyl-5a,5b,8,8,11a-pentamethyl-2-oxo-3,3a,4,5,5a,5b,6,7,7a,8,9,10,11,11a,11b,12,13,13a-octadecahydro-2H-cyclopenta[a]chrysen-3a-yl)-2-methylacrylic acid (1443513-41-4) → (E)-N-(1-(4-chlorophenyl)cyclopropyl)-3-((3aS,5aR,5bR,7aR,9S,11aR,11bR,13aS)-9-hydroxy-1-isopropyl-5a,5b,8,8,11a-pentamethyl-2-oxo-3,3a,4,5,5a,5b,6,7,7a,8,9,10,11,11a,11b,12,13,13a-octadecahydro-2H-cyclopenta[a]chrysen-3a-yl)-2-methylacrylamide (1443513-43-6)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 1h;

upstream raw materials:

4-Cyanochlorobenzene

ethylmagnesium bromide

Downstream raw materials:

5-(3-(1-(4-chlorophenyl)cyclopropylcarbamoyl)phenyl)-2-(4-fluorophenyl)-N-methylbenzofuran-3-carboxamide

methyl 4-(4-(1-(4-chlorophenyl)cyclopropylamino)-6-(2,2,2-trifluoroethoxy)-1,3,5-triazin-2-ylamino)benzoate

4-(4-(1-(4-chlorophenyl)cyclopropylamino)-6-(2,2,2-trifluoroethoxy)-1,3,5-triazin-2-ylamino)benzenesulfonamide

(E)-N-(1-(4-chlorophenyl)cyclopropyl)-3-((3aS,5aR,5bR,7aR,9S,11aR,11bR,13aS)-9-hydroxy-1-isopropyl-5a,5b,8,8,11a-pentamethyl-2-oxo-3,3a,4,5,5a,5b,6,7,7a,8,9,10,11,11a,11b,12,13,13a-octadecahydro-2H-cyclopenta[a]chrysen-3a-yl)-2-methylacrylamide

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