3-Chloro-naphthalenecarbaldehyde

Base Information

Chemical Name:3-Chloro-naphthalenecarbaldehyde
CAS No.:58782-64-2
Molecular Formula:C11H7ClO
Molecular Weight:190.62568
Hs Code.:
DSSTox Substance ID:DTXSID60595487
Wikidata:Q82490495
Mol file:58782-64-2.mol

Synonyms:58782-64-2;3-chloro-naphthalenecarbaldehyde;3-Chloronaphthalene-1-carboxaldehyde;3-chloro-1-naphthaldehyde;3-Chloronaphthalene-1-carbaldehyde;SCHEMBL2769437;DTXSID60595487;OAPWTWWAAZUPCK-UHFFFAOYSA-N;3-chloro-1-naphthalenecarbaldehyde;3-chloro-naphthalene-1-carbaldeyde;3-chloro naphthalene-1-carbaldehyde;3-Chloro-naphthalene-1-carbaldehyde;DB-083750;A936682

Suppliers and Price of 3-Chloro-naphthalenecarbaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 3-Chloro-naphthalenecarbaldehyde

Chemical Property:

PSA：17.07000
LogP:3.30570
XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:190.0185425
Heavy Atom Count:13
Complexity:193

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C=C(C=C2C=O)Cl

Technology Process of 3-Chloro-naphthalenecarbaldehyde

There total 4 articles about 3-Chloro-naphthalenecarbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 303779-69-3
1-(bromomethyl)-3-chloronaphthalene

: 58782-64-2
3-chloro-1-naphthaldehyde

Guidance literature:: With trimethylamine-N-oxide; In dichloromethane; dimethyl sulfoxide; at 20 ℃; for 6h;
DOI:10.1021/acs.orglett.0c03701

Reference yield:

: 104415-92-1
2-chloro-4-methylnaphthalene

: 58782-64-2
3-chloro-1-naphthaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 12 h / Reflux

2: trimethylamine-N-oxide / dimethyl sulfoxide; dichloromethane / 6 h / 20 °C

With N-Bromosuccinimide; trimethylamine-N-oxide; dibenzoyl peroxide; In tetrachloromethane; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/acs.orglett.0c03701