3-(1-ADAMANTYL)PENTANE-2,4-DIONE

Base Information

• Chemical Name: 3-(1-ADAMANTYL)PENTANE-2,4-DIONE
• CAS No.: 102402-84-6
• Molecular Formula: C15H22O2
• Molecular Weight: 234.338
• Hs Code.: 2914299000
• Mol file: 102402-84-6.mol

Synonyms:3-(1-ADAMANTYL)PENTANE-2,4-DIONE;2,4-pentanedione, 3-tricyclo[3.3.1.1~3,7~]dec-1-yl-;3-(1-adamantyl)pentane-2,4-dione(SALTDATA: FREE)

Chemical Property of 3-(1-ADAMANTYL)PENTANE-2,4-DIONE

Chemical Property:

• Vapor Pressure: 0.000116mmHg at 25°C
• Melting Point: 55-56℃
• Boiling Point: 335.9°C at 760 mmHg
• Flash Point: 126°C
• PSA: 34.14000
• Density: 1.097g/cm³
• LogP: 2.99700

Purity/Quality:

97% ^*data from raw suppliers

3-(1-adamantyl)pentane-2,4-dione ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-(1-ADAMANTYL)PENTANE-2,4-DIONE

There total 13 articles about 3-(1-ADAMANTYL)PENTANE-2,4-DIONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

1-Adamantyl bromide (768-90-1) + acetylacetone (123-54-6,81235-32-7) → 3-(adamantan-1-yl)pentane-2,4-dione (102402-84-6)

Guidance literature:

With iron(III)-acetylacetonate; at 110 ℃; for 6h; Reagent/catalyst; Concentration; Time; Temperature; Sealed tube;

DOI:10.1134/S1070428014100030

Reference yield: 81.0%

1-Adamantyl bromide (768-90-1) + bis(acetylacetonato)cobalt(II) (14024-48-7) → 3-(adamantan-1-yl)pentane-2,4-dione (102402-84-6)

Guidance literature:

In chlorobenzene; for 24h; Heating;

DOI:10.1016/S0040-4039(00)89236-9

Reference yield: 81.0%

1-Adamantyl bromide (768-90-1) → 3-(adamantan-1-yl)pentane-2,4-dione (102402-84-6)

Guidance literature:

In chlorobenzene; for 24h; Heating;

DOI:10.1016/S0040-4020(01)87650-X

upstream raw materials:

1-Adamantyl bromide

bis(acetylacetonato)cobalt(II)

1-adamanthanol

acetylacetone

Downstream raw materials:

4-(1-adamantyl)-3,5-dimethyl-1-phenylpyrazole

4-(1-adamantyl)-3,5-dimethylisoxazole

3,5-dimethyl-4-(1-adamantyl)pyrazole

1-(1-adamantyl)propan-2-one