6H-Purino[8,7-b][1,3]benzothiazine-2,4,6(1H,3H)-trione, 1,3-dimethyl-

Base Information

Chemical Name:6H-Purino[8,7-b][1,3]benzothiazine-2,4,6(1H,3H)-trione, 1,3-dimethyl-
CAS No.:205309-89-3
Molecular Formula:C14H10N4O3S
Molecular Weight:314.32
Hs Code.:
Mol file:205309-89-3.mol

Synonyms:6H-Purino[8,7-b][1,3]benzothiazine-2,4,6(1H,3H)-trione, 1,3-dimethyl-

Suppliers and Price of 6H-Purino[8,7-b][1,3]benzothiazine-2,4,6(1H,3H)-trione, 1,3-dimethyl-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6H-Purino[8,7-b][1,3]benzothiazine-2,4,6(1H,3H)-trione, 1,3-dimethyl-

Chemical Property:

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Technology Process of 6H-Purino[8,7-b][1,3]benzothiazine-2,4,6(1H,3H)-trione, 1,3-dimethyl-

There total 5 articles about 6H-Purino[8,7-b][1,3]benzothiazine-2,4,6(1H,3H)-trione, 1,3-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 7.8%

: 10381-75-6
8-bromotheophylline

: 147-93-3
Thiosalicylic acid

: 205309-89-3
1,3-Dimethyl-1H-10-thia-1,3,4b,11-tetraaza-benzo[b]fluorene-2,4,5-trione

: 2-(1,3-Dimethyl-2,6-dioxo-2,3,6,7-tetrahydro-1H-purin-8-ylsulfanyl)-benzoic acid

Guidance literature:: With copper(I) bromide; potassium carbonate; In N,N-dimethyl-formamide; at 120 ℃; for 24h;
DOI:10.1002/jhet.5570350111

Reference yield: 6.4%

: 88-65-3
2-bromobenzoic-acid

: 1784-70-9
8-mercapto-1,3-dimethyl-1H-purine-2,6-(3H,7H)-dione

: 205309-89-3
1,3-Dimethyl-1H-10-thia-1,3,4b,11-tetraaza-benzo[b]fluorene-2,4,5-trione

: 2-(1,3-Dimethyl-2,6-dioxo-2,3,6,7-tetrahydro-1H-purin-8-ylsulfanyl)-benzoic acid

Guidance literature:: With copper(I) bromide; potassium carbonate; In N,N-dimethyl-formamide; at 120 ℃; for 24h;
DOI:10.1002/jhet.5570350111

Reference yield:

: 88-65-3
2-bromobenzoic-acid

: 205309-89-3
1,3-Dimethyl-1H-10-thia-1,3,4b,11-tetraaza-benzo[b]fluorene-2,4,5-trione

Guidance literature:: Multi-step reaction with 2 steps

1: 6.4 percent / K₂CO₂, Cu₂Br₂ / dimethylformamide / 24 h / 120 °C

2: dimethylformamide / Heating

With copper(I) bromide; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570350111