oleanolic acid 3-O-monoglucuronide

Base Information

• Chemical Name: oleanolic acid 3-O-monoglucuronide
• CAS No.: 108322-31-2
• Molecular Formula: C₃₆H₅₆O₉
• Molecular Weight: 632.835
• Mol file: 108322-31-2.mol

Synonyms:oleanolic acid 3-O-monoglucuronide

Chemical Property of oleanolic acid 3-O-monoglucuronide

Chemical Property:

• Vapor Pressure: 5.13E-26mmHg at 25°C
• Boiling Point: 750.8°C at 760 mmHg
• Flash Point: 228.6°C
• Density: 1.27g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of oleanolic acid 3-O-monoglucuronide

There total 9 articles about oleanolic acid 3-O-monoglucuronide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

momordin Id → 28-desglucosylchikusetsusaponin IVa (26020-14-4,108322-31-2) + oleanolic acid (508-02-1,6880-10-0,25499-90-5) + momordin Ic

Guidance literature:

With sulfuric acid; at 80 ℃; for 20h;

DOI:10.1016/0031-9422(88)80773-8

Reference yield: 9.0%

momordin Ie → 28-desglucosylchikusetsusaponin IVa (26020-14-4,108322-31-2) + oleanolic acid (508-02-1,6880-10-0,25499-90-5) + momordin I

Guidance literature:

With sulfuric acid;

DOI:10.1016/0031-9422(88)80773-8

Reference yield:

(3β)-17-carboxy-28-norolean-12-en-3-yl 3'-O-(β-D-xylopyranosyl)-β-D-glucuronide (96990-18-0) → Oleanolic acid (508-02-1) + calenduloside E (26020-14-4,108322-31-2)

Guidance literature:

With sulfuric acid; at 80 ℃; for 10h;

DOI:10.1055/s-2006-958134

upstream raw materials:

3-O-{[β-D-glucopyranosyl (1->2)]-[α-L-arabinopyranosyl (1->3)]-β-D-glucuronopyranosyl}oleanolic acid

chikusetsusaponin IVa

(3β)-17-carboxy-28-norolean-12-en-3-yl 3'-O-(β-D-xylopyranosyl)-β-D-glucuronide

saponin-C methylester

Downstream raw materials:

D-glucuronic acid

Oleanolic acid

androseptoside A

D-glucuronic acid

Refernces

• 1、 Romussi,Bignardi. "Constituents of Cupuliferae, X: Triterpene saponins from Fagus silvatica L.". . p. 153 - 158. Retrieved 1987.
• 2、 Kawamura, Noriaki,Watanabe, Hitoshi,Oshio, Haruji. "SAPONINS FROM ROOTS OF MOMORDICA COCHINCHINENSIS". . p. 3585 - 3592. Retrieved 1988.