Benzoyl Chloride-13C6

Base Information

Chemical Name:Benzoyl Chloride-13C6
CAS No.:266308-67-2
Molecular Formula:C7H5ClO
Molecular Weight:146.503
Hs Code.:
European Community (EC) Number:694-118-5
DSSTox Substance ID:DTXSID10437409
Wikidata:Q82252899

Synonyms:266308-67-2;Benzoyl Chloride-13C6;Benzoyl chloride-(ring-13C6);DTXSID10437409;Benzoyl chloride-(phenyl-13C6), 99 atom % 13C, 99% (CP)

Suppliers and Price of Benzoyl Chloride-13C6

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of Benzoyl Chloride-13C6

Chemical Property:

Density:1.262 g/mL at 25 °C
XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:146.0230215
Heavy Atom Count:9
Complexity:106

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(=O)Cl
Isomeric SMILES:[13CH]1=[13CH][13CH]=[13C]([13CH]=[13CH]1)C(=O)Cl

Technology Process of Benzoyl Chloride-13C6

There total 2 articles about Benzoyl Chloride-13C6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 125945-98-4,170703-36-3
benzoic-ring-¹³C₆ acid

: 266308-67-2
benzoyl-1,2,3,4,5,6-¹³C₆ chloride

Guidance literature:: With thionyl chloride; In toluene; for 8h; Reflux;
DOI:10.1002/jlcr.3518

Reference yield:

: 125770-94-7
[13C₆]acetophenone

: 266308-67-2
benzoyl-1,2,3,4,5,6-¹³C₆ chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 4.37 g / NaOBr / H₂O / 3 h

2: thionyl chloride / benzene / 3 h / Heating

With thionyl chloride; sodium hypobromide; In water; benzene; 1: Oxidation / 2: Chlorination;
DOI:10.1002/(SICI)1099-1344(20000315)43:3<283::AID-JLCR314>3.0.CO;2-F