N-(3,4-Dichlorophenyl)benzamide

Base Information

• Chemical Name: N-(3,4-Dichlorophenyl)benzamide
• CAS No.: 10286-75-6
• Molecular Formula: C13H9 Cl2 N O
• Molecular Weight: 266.127
• Hs Code.: 2924299090
• Mol file: 10286-75-6.mol

Synonyms:Benzanilide,3',4'-dichloro- (7CI,8CI); 3',4'-Dichlorobenzanilide;N-(3,4-Dichlorophenyl)benzamide; N-Benzoyl-3,4-dichloroaniline

Chemical Property of N-(3,4-Dichlorophenyl)benzamide

Chemical Property:

• Vapor Pressure: 0.00086mmHg at 25°C
• Melting Point: 145-146 °C
• Boiling Point: 304.7°Cat760mmHg
• PKA: 11.97±0.70(Predicted)
• Flash Point: 138.1°C
• PSA: 32.59000
• Density: 1.384g/cm³
• LogP: 4.62970

Purity/Quality:

98%,99%, ^*data from raw suppliers

3',4'-DICHLOROBENZANILIDE Aldrich ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-(3,4-Dichlorophenyl)benzamide

There total 9 articles about N-(3,4-Dichlorophenyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1-benzoylpyrrolidin-2-one (2399-66-8) + m,p-dichloroaniline (95-76-1) → N-(3,4-dichlorophenyl)benzamide (10286-75-6)

Guidance literature:

With di-tert-butyl peroxide; tetra-(n-butyl)ammonium iodide; In water; for 16h; Heating; Green chemistry;

DOI:10.1039/d1ob00967b

Reference yield: 94.0%

3-phenyl-5H-1,4,2-dioxazol-5-one (19226-36-9) + 3,4-dichlophenylboronic acid (151169-75-4) → N-(3,4-dichlorophenyl)benzamide (10286-75-6)

Guidance literature:

With iron(II) chloride; In 1,2-dichloro-ethane; at 40 ℃; for 16h; chemoselective reaction; Inert atmosphere; Irradiation;

DOI:10.1021/acscatal.1c04538

Reference yield: 88.0%

benzoyl chloride (98-88-4) + m,p-dichloroaniline (95-76-1) → N-(3,4-dichlorophenyl)benzamide (10286-75-6)

Guidance literature:

With triethylamine; In ethyl acetate; at 20 ℃;

DOI:10.1021/jm030863d

upstream raw materials:

3'-chloro-benzanilide

(3,4-Dichloranilino)phenyl-acetonitril

benzoyl chloride

m,p-dichloroaniline

Downstream raw materials:

3',4'-dichlorothiobenzanilide

m,p-dichloroaniline

benzyl alcohol

1-[(3,4-dichlorophenylimino)phenylmethyl]-3-ethylthiourea