2-Acetoxy-5-acetoxymethyl-1,3-di-tert-butylbenzene

Base Information

• Chemical Name: 2-Acetoxy-5-acetoxymethyl-1,3-di-tert-butylbenzene
• CAS No.: 13154-59-1
• Molecular Formula: C19H28O4
• Molecular Weight: 320.429
• Hs Code.: 2915390090
• Mol file: 13154-59-1.mol

Synonyms:2-Acetoxy-5-acetoxymethyl-1,3-di-tert-butylbenzene

Chemical Property of 2-Acetoxy-5-acetoxymethyl-1,3-di-tert-butylbenzene

Chemical Property:

• PSA: 52.60000
• LogP: 4.27000

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Acetoxy-5-acetoxymethyl-1,3-di-tert-butylbenzene

There total 2 articles about 2-Acetoxy-5-acetoxymethyl-1,3-di-tert-butylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.0%

2,6-di-tert-butyl-4-hydroxy-4-methylcyclohexa-2,5-dienone (10396-80-2) + acetic anhydride (108-24-7) → 4-acetoxy-3,5-di-t-butylbenzyl acetate (13154-59-1) + 4-hydroxymethyl-2,6-di-t-butylphenyl acetate (83638-62-4)

Guidance literature:

With sulfuric acid; for 24h; Ambient temperature;

Reference yield:

→ 4-acetoxy-3,5-di-t-butylbenzyl acetate (13154-59-1)

Guidance literature:

3,5-Di-tert.-butyl-4-hydroxy-benzyl-acetat, Ac2O/H2SO4;

Reference yield:

4-acetoxy-3,5-di-t-butylbenzyl acetate (13154-59-1) → 3,5-di-tert-butyl-4-hydroxybenzyl acetate (14387-17-8)

Guidance literature:

With sulfuric acid; acetic acid;

upstream raw materials:

2,6-di-tert-butyl-4-hydroxy-4-methylcyclohexa-2,5-dienone

acetic anhydride

Downstream raw materials:

3,5-di-tert-butyl-4-hydroxybenzyl acetate

4-hydroxymethyl-2,6-di-t-butylphenyl acetate

Refernces