3α-Chloro-5α-cholestan-6-one

Base Information

Chemical Name:3α-Chloro-5α-cholestan-6-one
CAS No.:21072-86-6
Molecular Formula:C27H45ClO
Molecular Weight:421.1
Hs Code.:
Mol file:21072-86-6.mol

Synonyms:(3R,5S,8S,9S,10R,13R,14S,17R)-3-Chloro-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-6-one;3α-Chlor-5α-cholestan-6-on;3α-Chlor-5α-cholestanon-(6);

Suppliers and Price of 3α-Chloro-5α-cholestan-6-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of 3α-Chloro-5α-cholestan-6-one

Chemical Property:

Melting Point:181.5 - 182.5 °C
Boiling Point:500.4±33.0 °C(Predicted)
PSA：17.07000
Density:1.02±0.1 g/cm3(Predicted)
LogP:7.89410

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3α-Chloro-5α-cholestan-6-one

There total 11 articles about 3α-Chloro-5α-cholestan-6-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13095-30-2,13095-33-5,68521-96-0,115728-82-0,142923-80-6
3β-chloro-5,6α-epoxy-5α-cholestane

: 1056-93-5,5837-41-2,21072-85-5,21072-86-6,22033-80-3
3β-chloro-5α-cholestan-6-one

: 4031-23-6
3β-chloro-6β-fluoro-5α-cholestan-5α-ol

: 131249-39-3
3β-chloro-5β,14β-dimethyl-18,19-bisnor-10α-cholest-13(17)-en-6α-ol

: 131249-40-6
3β-chloro-5β-methyl-19-nor-cholest-9(10)-en-6α-ol

Guidance literature:: With boron trifluoride diethyl etherate; In benzene; at 20 ℃; for 0.116667h;

Reference yield:

: 6217-29-4,95825-96-0
(10R,13R,17R)-3-Chloro-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-6-nitro-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene

: 1056-93-5,5837-41-2,21072-85-5,21072-86-6,22033-80-3
(5S,10R,13R,17R)-3-Chloro-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-6-one

Guidance literature:: Multi-step reaction with 2 steps

1: Zn dust, NH₃, MeOH / diethyl ether / 0.5 h / Ambient temperature

2: Zn, HCl

With hydrogenchloride; methanol; ammonia; zinc; In diethyl ether;