Cyclohexanethiol,5-methyl-2-(1-methylethyl)-,(1R,2R,5S)-(9CI)

Base Information

Chemical Name:Cyclohexanethiol,5-methyl-2-(1-methylethyl)-,(1R,2R,5S)-(9CI)
CAS No.:174757-27-8
Molecular Formula:C10H20S
Molecular Weight:172.33
Hs Code.:
Mol file:174757-27-8.mol

Synonyms:Cyclohexanethiol,5-methyl-2-(1-methylethyl)-,(1R,2R,5S)-(9CI)

Suppliers and Price of Cyclohexanethiol,5-methyl-2-(1-methylethyl)-,(1R,2R,5S)-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of Cyclohexanethiol,5-methyl-2-(1-methylethyl)-,(1R,2R,5S)-(9CI)

Chemical Property:

PSA：38.80000
LogP:3.37700

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Cyclohexanethiol,5-methyl-2-(1-methylethyl)-,(1R,2R,5S)-(9CI)

There total 5 articles about Cyclohexanethiol,5-methyl-2-(1-methylethyl)-,(1R,2R,5S)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 103532-45-2
(+)-neomenthyl thioacetate

: 174757-27-8,196622-67-0,223653-15-4,173006-99-0
(1S,3R,4R)-p-menthane-3-thiol

Guidance literature:: With lithium aluminium tetrahydride;
DOI:10.1021/jo00369a020

Reference yield:

: 2216-51-5
(-)-menthol

: 174757-27-8,196622-67-0,223653-15-4,173006-99-0
(1S,3R,4R)-p-menthane-3-thiol

Guidance literature:: Multi-step reaction with 3 steps

1: (C₂H₅)3N / diethyl ether / 0.33 h / -20 °C

2: 84 percent / dimethylformamide / 20 h / 55 °C

3: 76 percent / LiAlH₄

With lithium aluminium tetrahydride; triethylamine; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1021/jo00369a020

Reference yield:

: 142921-58-2
(1S,2R,5S)-(+)-menthol Mesylate

: 174757-27-8,196622-67-0,223653-15-4,173006-99-0
(1S,3R,4R)-p-menthane-3-thiol

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / dimethylformamide / 20 h / 55 °C

2: 76 percent / LiAlH₄

With lithium aluminium tetrahydride; In N,N-dimethyl-formamide;
DOI:10.1021/jo00369a020