1,3,4-OXADIAZOLE, 3-ACETYL-2,3-DIHYDRO-2,5-BIS(3,4,5-TRIMETHOXYPHENYL)-

Base Information

Chemical Name:1,3,4-OXADIAZOLE, 3-ACETYL-2,3-DIHYDRO-2,5-BIS(3,4,5-TRIMETHOXYPHENYL)-
CAS No.:913254-35-0
Molecular Formula:C₂₂H₂₆N₂O₈
Molecular Weight:446.457
Hs Code.:
Mol file:913254-35-0.mol

Synonyms:1,3,4-OXADIAZOLE, 3-ACETYL-2,3-DIHYDRO-2,5-BIS(3,4,5-TRIMETHOXYPHENYL)-

Suppliers and Price of 1,3,4-OXADIAZOLE, 3-ACETYL-2,3-DIHYDRO-2,5-BIS(3,4,5-TRIMETHOXYPHENYL)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
3-ACETYL-2,3-DIHYDRO-2,5-BIS-(3,4,5-TRIMETHOXYPHENYL)-1,3,4-OXADIAZOLE 95.00%
5MG
$ 501.24

Total 0 raw suppliers

Chemical Property of 1,3,4-OXADIAZOLE, 3-ACETYL-2,3-DIHYDRO-2,5-BIS(3,4,5-TRIMETHOXYPHENYL)-

Chemical Property:

Vapor Pressure:6.49E-12mmHg at 25°C
Boiling Point:544.5°C at 760 mmHg
Flash Point:283.1°C
PSA：97.28000
Density:1.26g/cm³
LogP:2.35080

Purity/Quality:: 3-ACETYL-2,3-DIHYDRO-2,5-BIS-(3,4,5-TRIMETHOXYPHENYL)-1,3,4-OXADIAZOLE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,3,4-OXADIAZOLE, 3-ACETYL-2,3-DIHYDRO-2,5-BIS(3,4,5-TRIMETHOXYPHENYL)-

There total 4 articles about 1,3,4-OXADIAZOLE, 3-ACETYL-2,3-DIHYDRO-2,5-BIS(3,4,5-TRIMETHOXYPHENYL)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 90754-75-9
3,4,5-trimethoxy-benzoic acid (3,4,5-trimethoxy-benzylidene)-hydrazide

: 108-24-7
acetic anhydride

: 913254-35-0
2-(3',4',5'-trimethoxyphenyl)-5-(3'',4'',5''-trimethoxyphenyl)-2-acetyl-2,3-dihydro-1,3,4-oxadiazoline

Guidance literature:: for 1h; Reflux;
DOI:10.1021/jm901268n

Reference yield: 67.3%

: C₂₀H₂₄N₂O₇

: 108-24-7
acetic anhydride

: 913254-35-0
2-(3',4',5'-trimethoxyphenyl)-5-(3'',4'',5''-trimethoxyphenyl)-2-acetyl-2,3-dihydro-1,3,4-oxadiazoline

Guidance literature:: for 2h; Heating;
DOI:10.1016/j.bmcl.2006.07.048

Reference yield:

: 86-81-7
3,4,5-trimethoxy-benzaldehyde

: 913254-35-0
2-(3',4',5'-trimethoxyphenyl)-5-(3'',4'',5''-trimethoxyphenyl)-2-acetyl-2,3-dihydro-1,3,4-oxadiazoline

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / ethanol / 0.5 h / Heating

2: 67.3 percent / 2 h / Heating

In ethanol;
DOI:10.1016/j.bmcl.2006.07.048