Technology Process of 1,1'-[(1,2-Dimethyl-1,2-ethanediyl)bis(oxymethylene)]bisbenzene
There total 2 articles about 1,1'-[(1,2-Dimethyl-1,2-ethanediyl)bis(oxymethylene)]bisbenzene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium hydroxide;
tetra(n-butyl)ammonium hydrogensulfate;
In
toluene;
at 50 ℃;
for 24h;
Product distribution;
selectivity of etherification with different prim., sec. and tert. diols;
DOI:10.1016/0040-4020(89)80151-6
- Guidance literature:
-
With
thallium (I) ethoxide;
Yield given. Multistep reaction. Yields of byproduct given;
1) MeCN, r.t., 2) MeCN, 20 deg C, 14 h;