N-[(Benzyloxy)carbonyl]-L-glutamic acid 5-methyl 1-(pentachlorophenyl) ester

Base Information

• Chemical Name: N-[(Benzyloxy)carbonyl]-L-glutamic acid 5-methyl 1-(pentachlorophenyl) ester
• CAS No.: 25613-46-1
• Molecular Formula: C₂₀H₁₆Cl₅NO₆
• Molecular Weight: 543.615
• Mol file: 25613-46-1.mol

Synonyms:N-[(Benzyloxy)carbonyl]-L-glutamic acid 5-methyl 1-(pentachlorophenyl) ester

Chemical Property of N-[(Benzyloxy)carbonyl]-L-glutamic acid 5-methyl 1-(pentachlorophenyl) ester

Chemical Property:

• Melting Point: 120 - 121 °C (ethanol)
• PSA: 90.93000
• LogP: 6.49810

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of N-[(Benzyloxy)carbonyl]-L-glutamic acid 5-methyl 1-(pentachlorophenyl) ester

There total 2 articles about N-[(Benzyloxy)carbonyl]-L-glutamic acid 5-methyl 1-(pentachlorophenyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Pentachlorophenol (87-86-5,67471-28-7) + (S)-2-Benzyloxycarbonylamino-pentanedioic acid 5-methyl ester (4652-65-7) → N-Carbobenzoxy-γ-methyl-L-glutaminsaeure-pentachlorphenylester (25613-46-1)

Guidance literature:

Multistep reaction; (i) 1-cyclohexyl-3-(2-morpholinoethyl)-carbodiimide metho-4-toluenesulfonate, CH₂Cl₂, (ii) /BRN= 1285380/;

DOI:10.1021/jo00954a020

Reference yield:

→ N-Carbobenzoxy-γ-methyl-L-glutaminsaeure-pentachlorphenylester (25613-46-1)

Guidance literature:

Z-γ-Methyl-L-glutamat(II) in CH2Cl2 , Dicyclohexylcarbodiimid, Pentachlorphenol und CH3COOH;

Reference yield:

N-Carbobenzoxy-γ-methyl-L-glutaminsaeure-pentachlorphenylester (25613-46-1) → 2-Benzyloxycarbonylamino-pentanedioic acid 5-methyl ester 1-pentachlorophenyl ester (39994-03-1)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 23 ℃; Rate constant;

DOI:10.1021/jo00954a020

upstream raw materials:

Pentachlorophenol

(S)-2-Benzyloxycarbonylamino-pentanedioic acid 5-methyl ester

Downstream raw materials:

N-Benzyloxycarbonyl-α-L-glutamyl-(γ-methylester)-L-valinmethylester

2-Benzyloxycarbonylamino-pentanedioic acid 5-methyl ester 1-pentachlorophenyl ester

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