1-(3-Cyanopropyl)pyridinium bis(trifluoromethylsulfonyl)imide

Base Information

• Chemical Name: 1-(3-Cyanopropyl)pyridinium bis(trifluoromethylsulfonyl)imide
• CAS No.: 820972-37-0
• Molecular Formula: C₂F₆NO₄S₂*C₉H₁₁N₂
• Molecular Weight: 427.348
• Mol file: 820972-37-0.mol

Synonyms:1-(3-Cyanopropyl)pyridinium bis(trifluoromethylsulfonyl)imide

Chemical Property of 1-(3-Cyanopropyl)pyridinium bis(trifluoromethylsulfonyl)imide

Chemical Property:

• Refractive Index: n20/D 1.458±0.001
• PSA: 112.71000
• LogP: 4.49878

Purity/Quality:

1-(3-CYANOPROPYL)PYRIDINIUM BIS(TRIFLUOROMETHYLSULFONYL)IMIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(3-Cyanopropyl)pyridinium bis(trifluoromethylsulfonyl)imide

There total 3 articles about 1-(3-Cyanopropyl)pyridinium bis(trifluoromethylsulfonyl)imide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Br(1-)*C9H11N2(1+) (64480-46-2) + bis(trifluoromethane)sulfonimide lithium (90076-65-6) → N-butyronitrile-pyridinium bis(trifluoromethylsulfonyl)imide (820972-37-0)

Guidance literature:

In water;

DOI:10.1021/jp2027675

Reference yield:

pyridine (110-86-1) → N-butyronitrile-pyridinium bis(trifluoromethylsulfonyl)imide (820972-37-0)

Guidance literature:

DOI:10.1055/s-2006-944198

Reference yield:

bis(trifluoromethane)sulfonimide lithium (90076-65-6) + 4-butyronitrilepyridinium chloride (820972-34-7) → N-butyronitrile-pyridinium bis(trifluoromethylsulfonyl)imide (820972-37-0)

Guidance literature:

DOI:10.1055/s-2006-944198

upstream raw materials:

bis(trifluoromethane)sulfonimide lithium

4-butyronitrilepyridinium chloride

pyridine

Br^(1-)*C₉H₁₁N₂⁽¹⁺⁾

Refernces

• 1、 Dubbaka, Srinivas Reddy,Zhao, Dongbin,Fei, Zhaofu,Volla, Chandra M. Rao,Dyson, Paul J.,Vogel, Pierre. "Palladium-catalyzed desulfitative Mizoroki-Heck coupling reactions of sulfonyl chlorides with olefins in a nitrile-functionalized ionic liquid". . p. 3155 - 3157. Retrieved 2008/02/13.