4-methoxy-2,3,5-trimethylbenzenesulfonyl chloride(SALTDATA: FREE)

Base Information

• Chemical Name: 4-methoxy-2,3,5-trimethylbenzenesulfonyl chloride(SALTDATA: FREE)
• CAS No.: 1016500-29-0
• Molecular Formula: C10H13ClO3S
• Molecular Weight: 248.73
• Hs Code.: 2909309090
• Mol file: 1016500-29-0.mol

Synonyms:4-methoxy-2,3,5-trimethylbenzenesulfonyl chloride(SALTDATA: FREE)

Chemical Property of 4-methoxy-2,3,5-trimethylbenzenesulfonyl chloride(SALTDATA: FREE)

Chemical Property:

• PSA: 51.75000
• LogP: 3.62870

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-methoxy-2,3,5-trimethylbenzenesulfonyl chloride(SALTDATA: FREE)

There total 1 articles about 4-methoxy-2,3,5-trimethylbenzenesulfonyl chloride(SALTDATA: FREE) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

1-methoxy-2,3,6-trimethylbenzene (21573-36-4) → 4-methoxy-2,3,5-trimethylbenzene-1-sulfonyl chloride (1016500-29-0)

Guidance literature:

With chlorosulfonic acid; In dichloromethane; at 0 - 20 ℃;

Reference yield: 95.0%

(2-hydroxyethyl)(methyl)amine (109-83-1) + 4-methoxy-2,3,5-trimethylbenzene-1-sulfonyl chloride (1016500-29-0) → N-(2-hydroxyethyl)-4-methoxy-N,2,3,5-tetramethylbenzenesulfonamide (1174284-29-7)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; for 3h;

Reference yield: 83.0%

4-methoxy-2,3,5-trimethylbenzene-1-sulfonyl chloride (1016500-29-0) + C9H15N3*ClH (1185293-78-0) → 3-(1H-imidazol-1-ylmethyl)-1-[(4-methoxy-2,3,5-trimethylphenyl)sulfonyl]piperidine

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; for 96h;

DOI:10.1016/j.bmcl.2016.04.078

upstream raw materials:

1-methoxy-2,3,6-trimethylbenzene

Downstream raw materials:

N-(2-hydroxyethyl)-4-methoxy-N,2,3,5-tetramethylbenzenesulfonamide

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