2,3-dehydrodeoxamuscarine

Base Information

Chemical Name:2,3-dehydrodeoxamuscarine
CAS No.:79195-20-3
Molecular Formula:C₁₀H₂₀NO*I
Molecular Weight:297.179
Hs Code.:
Mol file:79195-20-3.mol

Synonyms:2,3-dehydrodeoxamuscarine

Suppliers and Price of 2,3-dehydrodeoxamuscarine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 3 raw suppliers

Chemical Property of 2,3-dehydrodeoxamuscarine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 2,3-dehydrodeoxamuscarine

There total 21 articles about 2,3-dehydrodeoxamuscarine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: trans-3-methyl-4-hydroxy-1-(N,N-dimethylaminomethyl)cyclopent-2-ene

: 74-88-4
methyl iodide

: 79195-20-3
trans-2,3-dehydrodeoxamuscarine

Guidance literature:: In diethyl ether; Ambient temperature;
DOI:10.1002/jps.2600700506

Reference yield:

: 3-methyl-4-oxo-1-carbomethoxycyclopent-2-ene

: 79195-20-3
cis-2,3-dehydrodeoxamuscarine

Guidance literature:: Multi-step reaction with 4 steps

1: 0.42 g / 9-borabicyclo<3.3.1>nonane / tetrahydrofuran / 1) 0 deg C, 4 h; 2) 25 deg C, 2 h

2: 0.25 g / 48 h / 95 - 100 °C

3: 0.26 g / LiAlH₄ / tetrahydrofuran / 5 h / Heating

4: 0.23 g / diethyl ether / Ambient temperature

With lithium aluminium tetrahydride; 9-borabicyclo[3.3.1]nonane dimer; In tetrahydrofuran; diethyl ether;
DOI:10.1002/jps.2600700506

Reference yield:

: 3-methyl-4-oxo-1-carbomethoxycyclopent-2-ene

: 79195-20-3
trans-2,3-dehydrodeoxamuscarine

Guidance literature:: Multi-step reaction with 6 steps

1: 0.42 g / 9-borabicyclo<3.3.1>nonane / tetrahydrofuran / 1) 0 deg C, 4 h; 2) 25 deg C, 2 h

2: 0.25 g / 48 h / 95 - 100 °C

3: 0.26 g / LiAlH₄ / tetrahydrofuran / 5 h / Heating

4: 1.0 g / chromium trioxide, aq. H₂SO₄ / 2 h / Ambient temperature

5: 0.35 g / 9-borabicyclo<3.3.1>nonane / tetrahydrofuran / 1) 0 deg C, 4 h; 2) 25 deg C, 2 h

6: 85 percent / diethyl ether / Ambient temperature

With chromium(VI) oxide; lithium aluminium tetrahydride; 9-borabicyclo[3.3.1]nonane dimer; sulfuric acid; In tetrahydrofuran; diethyl ether;
DOI:10.1002/jps.2600700506