Carbamic acid, (2,3-diaminopropyl)-, 1,1-dimethylethyl ester (9CI)

Base Information

Chemical Name:Carbamic acid, (2,3-diaminopropyl)-, 1,1-dimethylethyl ester (9CI)
CAS No.:163133-92-4
Molecular Formula:C₈H₁₉N₃O₂
Molecular Weight:189.258
Hs Code.:
Mol file:163133-92-4.mol

Synonyms:Carbamic acid, (2,3-diaminopropyl)-, 1,1-dimethylethyl ester (9CI);tert-butyl 2,3-diaminopropylcarbamate

Suppliers and Price of Carbamic acid, (2,3-diaminopropyl)-, 1,1-dimethylethyl ester (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
tert-butylN-(2,3-diaminopropyl)carbamate
5mg
$ 65.00

AK Scientific
Tert-Butyl(2,3-diaminopropyl)carbamate
1g
$ 1429.00

Total 2 raw suppliers

Chemical Property of Carbamic acid, (2,3-diaminopropyl)-, 1,1-dimethylethyl ester (9CI)

Chemical Property:

Boiling Point:331.9±32.0 °C(Predicted)
PKA:12.34±0.46(Predicted)
Density:1.047±0.06 g/cm3(Predicted)

Purity/Quality:

98%min ^*data from raw suppliers

tert-butylN-(2,3-diaminopropyl)carbamate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Carbamic acid, (2,3-diaminopropyl)-, 1,1-dimethylethyl ester (9CI)

There total 6 articles about Carbamic acid, (2,3-diaminopropyl)-, 1,1-dimethylethyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 190840-29-0
1,2-diazido-3-(BOC-amino)propane

: 163133-92-4
1,2-diamino-3-(BOC-amino)propane

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; under 2250.2 Torr;
DOI:10.1055/s-1998-2128

Reference yield: 90.0%

: 213475-69-5
(2-Benzyloxycarbonylamino-3-tert-butoxycarbonylamino-propyl)-carbamic acid benzyl ester

: 163133-92-4
1,2-diamino-3-(BOC-amino)propane

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; under 750.06 Torr;
DOI:10.1055/s-1998-2128

Reference yield:

: 137618-48-5
tert-butyl N-(2,3-dihydroxypropyl)carbamate

: 163133-92-4
1,2-diamino-3-(BOC-amino)propane

Guidance literature:: Multi-step reaction with 3 steps

1: 69 percent / Et₃N / CH₂Cl₂ / 1.) 0 deg C, 1 h, 2.) r.t., 30 min

2: 69 percent / NaN₃, 15-crown-5 / dimethylformamide / 12 h / 60 - 70 °C

3: 99 percent / H₂ / 5percent Pd/C / methanol / 2250.2 Torr

With sodium azide; 15-crown-5; hydrogen; triethylamine; palladium on activated charcoal; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1055/s-1998-2128