9(S)-HODE CHOLESTERYL ESTER

Base Information

• Chemical Name: 9(S)-HODE CHOLESTERYL ESTER
• CAS No.: 143442-54-0
• Molecular Formula: C45H76O3
• Molecular Weight: 665.08
• Mol file: 143442-54-0.mol

Synonyms:9(S)-HODE CHOLESTERYL ESTER;9S-HYDROXY-10E,12Z-OCTADECADIENOIC ACID, CHOLESTERYL ESTER

Chemical Property of 9(S)-HODE CHOLESTERYL ESTER

Chemical Property:

• PSA: 46.53000
• LogP: 12.72390

Purity/Quality:

99% ^*data from raw suppliers

9(S)-HODE cholesteryl ester ≥98% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 9(S)-HODE CHOLESTERYL ESTER

There total 4 articles about 9(S)-HODE CHOLESTERYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cholesterol linoleate (604-33-1) → (8E,12Z)-10-Hydroxy-octadeca-8,12-dienoic acid (3S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester + cholesteryl 13-hydroxyoctadeca-cis-9,trans-11-dienoate (167354-91-8) + cholesteryl 9-hydroxyoctadeca-trans-10,cis-12-dienoate (33783-76-5,143442-54-0,330800-93-6) + (9Z,13E)-12-Hydroxy-octadeca-9,13-dienoic acid (3S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester

Guidance literature:

cholesterol linoleate; With oxygen; methylene blue; In hexane; isopropyl alcohol; at 4 ℃; for 5h; Irradiation;

With potassium iodide; In ethanol; at 20 ℃; for 1h; Title compound not separated from byproducts;

DOI:10.1016/S0009-3084(99)00049-3

Reference yield:

cholesterol 9-hydroperoxy-trans-10,cis-12-octadecadienoate (176181-03-6) → cholesteryl 9-hydroxyoctadeca-trans-10,cis-12-dienoate (33783-76-5,143442-54-0,330800-93-6)

Guidance literature:

With triphenylphosphine; In diethyl ether;

DOI:10.1021/tx9600098

Reference yield:

cholesteryl 9-hydroperoxyoctadeca-trans-10,trans-12-dienoate (176300-84-8) → cholesteryl 9-hydroxyoctadeca-trans-10,trans-12-dienoate (143442-54-0,330800-93-6)

Guidance literature:

With triphenylphosphine; In diethyl ether;

DOI:10.1021/tx9600098

upstream raw materials:

cholesterol linoleate

cholesterol 9-hydroperoxy-trans-10,cis-12-octadecadienoate

cholesteryl 9-hydroperoxyoctadeca-trans-10,trans-12-dienoate