(R,S)-1-Tosyl Glycerol-d5

Base Information

• Chemical Name: (R,S)-1-Tosyl Glycerol-d5
• CAS No.: 928623-32-9
• Molecular Formula: C10H9D5O5S
• Molecular Weight: 251.244
• Mol file: 928623-32-9.mol

Synonyms:(R,S)-1-Tosyl Glycerol-d5;1,2,3-Propanetriol 1-(4-Methylbenzenesulfonate)-d5;1-p-Toluenesulfonate Glycerol-d5;1-Tosyloxy-2,3-propanediol-d5;2,3-Dihydroxypropyl Tosylate-d5;p-Toluenesulfonic Acid Glyceryl Ester-d5

Chemical Property of (R,S)-1-Tosyl Glycerol-d5

Chemical Property:

• PSA: 92.21000
• LogP: 1.13430
• Solubility.: Acetone, Chloroform,

Purity/Quality:

97% ^*data from raw suppliers

(R,S)-1-TosylGlycerol-d5 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: Protected, labelled Glycerol.

Technology Process of (R,S)-1-Tosyl Glycerol-d5

There total 1 articles about (R,S)-1-Tosyl Glycerol-d5 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

allyl-d5 4-methylbenzenesulfonate (185201-66-5) → 2,3-dihydroxypropyl 4-methylbenzenesulfonate-d5 (928623-32-9)

Guidance literature:

allyl-d5 4-methylbenzenesulfonate; With AD-mix-β; water; tert-butyl alcohol; at 0 ℃; for 18h;

With sodium hydrogensulfite; In water; tert-butyl alcohol; at 0 - 20 ℃; for 1h;

Reference yield:

2,3-dihydroxypropyl 4-methylbenzenesulfonate-d5 (928623-32-9) + N,N'-bis(2,3-dihydroxypropyl)-5-acetamido-2,4,6-triiodoisophthalamide (31127-80-7) → 5-(acetyl(2,3-dihydroxypropyl)amino)-N,N'-bis(2,3-dihydroxypropyl)-2,4,6-triiodo-1,3-benzenedicarboxamide-d5

Guidance literature:

N,N'-bis(2,3-dihydroxypropyl)-5-acetamido-2,4,6-triiodoisophthalamide; With calcium hydroxide; sodium hydroxide; In water; at 85 ℃; for 0.5h;

2,3-dihydroxypropyl 4-methylbenzenesulfonate-d₅; In water; for 0.5h;

upstream raw materials:

allyl-d5 4-methylbenzenesulfonate

Refernces