benzyl 2-aMinopropylcarbaMate

Base Information

• Chemical Name: benzyl 2-aMinopropylcarbaMate
• CAS No.: 84477-88-3
• Molecular Formula: C11H16N2O2
• Molecular Weight: 208.25694
• Mol file: 84477-88-3.mol

Synonyms:benzyl 2-aMinopropylcarbaMate;N-(2-Aminopropyl)carbamic acid phenylmethyl ester

Chemical Property of benzyl 2-aMinopropylcarbaMate

Chemical Property:

• PSA: 64.35000
• Density: 1.107
• LogP: 2.35120

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of benzyl 2-aMinopropylcarbaMate

There total 2 articles about benzyl 2-aMinopropylcarbaMate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

benzyl phenyl carbonate (28170-07-2) + 1,2-diaminopropan (78-90-0,10424-38-1) → 1-(benzyloxycarbonyl) amino-2-aminopropane (84477-88-3,934660-64-7,934660-63-6)

Guidance literature:

In ethanol; at 20 ℃;

DOI:10.1055/s-2002-34859

Reference yield:

benzyl chloroformate (501-53-1,94274-21-2) + 1,2-diaminopropan (78-90-0,10424-38-1) → 1-(benzyloxycarbonyl) amino-2-aminopropane (84477-88-3,934660-64-7,934660-63-6)

Guidance literature:

benzyl chloroformate; 1,2-diaminopropan; With triethylamine; In dehydrated diethyl ether; at 0 ℃; for 18h;

In ethyl acetate;

Reference yield:

acryloyl chloride (814-68-6,25189-84-8) + 1-(benzyloxycarbonyl) amino-2-aminopropane (84477-88-3,934660-64-7,934660-63-6) → 2-(benzyloxycarbonyl)aminoisopropyl acrylamide

Guidance literature:

acryloyl chloride; 1-(benzyloxycarbonyl) amino-2-aminopropane; With triethylamine; In diethyl ether; for 2h;

In ethyl acetate;

upstream raw materials:

benzyl phenyl carbonate

1,2-diaminopropan

benzyl chloroformate

Refernces

• 1、 -. "ACRYLAMIDE DERIVATIVES AND POLYMERS CONTAINING SAID DERIVATIVES". Page 9-10. . Retrieved 2010/02/06.