2-Iodo-1-methoxynaphthalene

Base Information

• Chemical Name: 2-Iodo-1-methoxynaphthalene
• CAS No.: 151560-43-9
• Molecular Formula: C11H9IO
• Molecular Weight: 284.096
• DSSTox Substance ID: DTXSID80446967
• Nikkaji Number: J562.490H
• Wikidata: Q82265725
• Mol file: 151560-43-9.mol

Synonyms:2-Iodo-1-methoxynaphthalene;151560-43-9;DTXSID80446967;FT-0719068

Chemical Property of 2-Iodo-1-methoxynaphthalene

Chemical Property:

• PSA: 9.23000
• LogP: 3.45300
• XLogP3: 3.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 1
• Exact Mass: 283.96981
• Heavy Atom Count: 13
• Complexity: 172

Purity/Quality:

98% ^*data from raw suppliers

2-Iodo-1-methoxynaphthalene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=C(C=CC2=CC=CC=C21)I

Technology Process of 2-Iodo-1-methoxynaphthalene

There total 6 articles about 2-Iodo-1-methoxynaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1-Methoxynaphthalene (2216-69-5) → 2-Iodo-1-methoxynaphthalene (151560-43-9)

Guidance literature:

With sodium periodate; potassium iodide; sodium chloride; In water; acetic acid; at 25 ℃; for 8h;

DOI:10.1016/j.tetlet.2006.05.062

Reference yield: 49.0%

1-Methoxynaphthalene (2216-69-5) → 1-iodo-4-methoxynaphthalene (2607-25-2) + 2-Iodo-1-methoxynaphthalene (151560-43-9)

Guidance literature:

With Oxone; potassium iodide; In methanol; at 20 ℃; for 24h;

DOI:10.1081/SCC-120006002

Reference yield: 9.0%

1-Methoxynaphthalene (2216-69-5) → 8-iodo-1-methoxy-naphthalene (5783-59-5) + 2-Iodo-1-methoxynaphthalene (151560-43-9)

Guidance literature:

With iodine; tert.-butyl lithium; In diethyl ether; pentane; at 20 ℃; for 4h;

DOI:10.1021/jo000684t

upstream raw materials:

1-methoxynaphthalen-2-amine

1-Methoxynaphthalene

2-nitro-1-methoxynaphthalene

Downstream raw materials:

2,2'-binaphthol

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