tert-butyl 2-(4,4-difluorocyclohexyl)hydrazinecarboxylate

Base Information

Chemical Name:tert-butyl 2-(4,4-difluorocyclohexyl)hydrazinecarboxylate
CAS No.:1214910-72-1
Molecular Formula:C11H20F2N2O2
Molecular Weight:250.289
Hs Code.:
Mol file:1214910-72-1.mol

Synonyms:tert-butyl 2-(4,4-difluorocyclohexyl)hydrazinecarboxylate

Suppliers and Price of tert-butyl 2-(4,4-difluorocyclohexyl)hydrazinecarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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price

Total 4 raw suppliers

Chemical Property of tert-butyl 2-(4,4-difluorocyclohexyl)hydrazinecarboxylate

Chemical Property:

PSA：50.36000
Density:1.12±0.1 g/cm3(Predicted)
LogP:3.37540

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of tert-butyl 2-(4,4-difluorocyclohexyl)hydrazinecarboxylate

There total 4 articles about tert-butyl 2-(4,4-difluorocyclohexyl)hydrazinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 870-46-2
t-butoxycarbonylhydrazine

: 22515-18-0
4,4-difluorocyclohexanone

: 1214910-72-1
N'-(4,4-difluorocyclohexyl)hydrazinecarboxylic acid tert-butyl ester

Guidance literature:: With hydrogen; acetic acid; platinum(IV) oxide; In isopropyl alcohol; at 20 ℃; for 12h; under 2585.81 Torr;

Reference yield: 84.0%

: N'-(4,4-difluorocyclohexylidene)hydrazinecarboxylic acid tert-butyl ester

: 1214910-72-1
N'-(4,4-difluorocyclohexyl)hydrazinecarboxylic acid tert-butyl ester

Guidance literature:: With sodium tris(acetoxy)borohydride; In tetrahydrofuran; at 20 ℃; for 15h;

Reference yield:

: 870-46-2
t-butoxycarbonylhydrazine

: 1214910-72-1
N'-(4,4-difluorocyclohexyl)hydrazinecarboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 1 h / 20 °C

2: palladium on activated charcoal; hydrogen / methanol / 16 h / 40 °C / 7500.75 Torr

With palladium on activated charcoal; hydrogen; In methanol;