CarbaMic acid, N-[3-broMo-1-[(4-Methylphenyl)sulfonyl]-1H-pyrrolo[2,3-b]pyridin-5-yl]-, phenylMethyl ester

Base Information

Chemical Name:CarbaMic acid, N-[3-broMo-1-[(4-Methylphenyl)sulfonyl]-1H-pyrrolo[2,3-b]pyridin-5-yl]-, phenylMethyl ester
CAS No.:1036028-08-6
Molecular Formula:C22H18BrN3O4S
Molecular Weight:500.373
Hs Code.:

Synonyms:CarbaMic acid, N-[3-broMo-1-[(4-Methylphenyl)sulfonyl]-1H-pyrrolo[2,3-b]pyridin-5-yl]-, phenylMethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of CarbaMic acid, N-[3-broMo-1-[(4-Methylphenyl)sulfonyl]-1H-pyrrolo[2,3-b]pyridin-5-yl]-, phenylMethyl ester

Chemical Property:

PSA：102.16000
LogP:6.18730

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of CarbaMic acid, N-[3-broMo-1-[(4-Methylphenyl)sulfonyl]-1H-pyrrolo[2,3-b]pyridin-5-yl]-, phenylMethyl ester

There total 1 articles about CarbaMic acid, N-[3-broMo-1-[(4-Methylphenyl)sulfonyl]-1H-pyrrolo[2,3-b]pyridin-5-yl]-, phenylMethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1036028-07-5
benzyl 3-bromo-1H-pyrrolo[2,3-b]pyridin-5-ylcarbamate

: 98-59-9
p-toluenesulfonyl chloride

: 1036028-08-6
benzyl 3-bromo-1-tosyl-1H-pyrrolo[2,3-b]pyridin-5-ylcarbamate

Guidance literature:: benzyl 3-bromo-1H-pyrrolo[2,3-b]pyridin-5-ylcarbamate; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 1h;

p-toluenesulfonyl chloride; In tetrahydrofuran; at 0 - 20 ℃; for 4.16667h;

With water; ammonium chloride; In tetrahydrofuran;

Reference yield: 73.0%

: 1036028-08-6
benzyl 3-bromo-1-tosyl-1H-pyrrolo[2,3-b]pyridin-5-ylcarbamate

: 73183-34-3
bis(pinacol)diborane

: 1036028-09-7
benzyl 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-tosyl-1H-pyrrolo[2,3-b]pyridin-5-ylcarbamate

Guidance literature:: benzyl 3-bromo-1-tosyl-1H-pyrrolo[2,3-b]pyridin-5-ylcarbamate; bis(pinacol)diborane; With potassium acetate; In 1,4-dioxane; for 0.333333h;

tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; for 2h; Heating / reflux;