N-Cbz-N-Methyl-b-alanine

Base Information

Chemical Name:N-Cbz-N-Methyl-b-alanine
CAS No.:121148-97-8
Molecular Formula:C12H15NO4
Molecular Weight:237.255
Hs Code.:
Mol file:121148-97-8.mol

Synonyms:N-Cbz-N-Methyl-b-alanine

Suppliers and Price of N-Cbz-N-Methyl-b-alanine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
3-((Benzyloxycarbonyl)(methyl)amino)propanoicAcid
100mg
$ 220.00

Crysdot
3-(((Benzyloxy)carbonyl)(methyl)amino)propanoicacid 95+%
1g
$ 371.00

Chemenu
3-(((benzyloxy)carbonyl)(methyl)amino)propanoicacid 95%
1g
$ 351.00

AK Scientific
3-([(Benzyloxy)carbonyl](methyl)amino)propanoicacid
100mg
$ 374.00

AK Scientific
3-([(Benzyloxy)carbonyl](methyl)amino)propanoicacid
10g
$ 2182.00

AK Scientific
3-([(Benzyloxy)carbonyl](methyl)amino)propanoicacid
5g
$ 1234.00

Acrotein
N-Cbz-N-methyl-b-alanine 97%
5g
$ 495.00

Total 4 raw suppliers

Chemical Property of N-Cbz-N-Methyl-b-alanine

Chemical Property:

PSA：66.84000
LogP:1.72970

Purity/Quality:

97% ^*data from raw suppliers

3-((Benzyloxycarbonyl)(methyl)amino)propanoicAcid ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-Cbz-N-Methyl-b-alanine

There total 4 articles about N-Cbz-N-Methyl-b-alanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 922705-65-5
phenylmethyl (3-diazo-2-oxopropyl)methylcarbamate

: 121148-97-8
3-(methyl{[(phenylmethyl)oxy]carbonyl}amino)propanoic acid

Guidance literature:: With silver trifluoroacetate; In 1,4-dioxane; water; for 0.5h; sonication;
DOI:10.1002/hlca.200690235

Reference yield: 50.0%

: 922705-29-1
phenylmethyl 6-oxo-1,3-oxazinane-3-carboxylate

: 121148-97-8
3-(methyl{[(phenylmethyl)oxy]carbonyl}amino)propanoic acid

Guidance literature:: With triethylsilane; trifluoroacetic acid; In dichloromethane;
DOI:10.1002/hlca.200690235

Reference yield:

: 55740-06-2
phenylmethyl 5-oxo-1,3-oxazolidine-3-carboxylate

: 121148-97-8
3-(methyl{[(phenylmethyl)oxy]carbonyl}amino)propanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: Et₃SiH; CF₃COOH / CH₂Cl₂

2.1: ClCOOEt; N-methylmorpholine / tetrahydrofuran / 0.25 h / -15 °C

2.2: 65 percent / tetrahydrofuran; CH₂Cl₂ / -15 - 20 °C

3.1: 70 percent / CF₃COOAg / dioxane; H₂O / 0.5 h / sonication

With 4-methyl-morpholine; triethylsilane; silver trifluoroacetate; chloroformic acid ethyl ester; trifluoroacetic acid; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; 3.1: Wolff rearrangement;
DOI:10.1002/hlca.200690235