α-Chlorobenzenebutanenitrile

Base Information

Chemical Name:α-Chlorobenzenebutanenitrile
CAS No.:53279-93-9
Molecular Formula:C₁₀H₁₀ClN
Molecular Weight:179.649
Hs Code.:
Mol file:53279-93-9.mol

Synonyms:α-Chlorobenzenebutanenitrile

Suppliers and Price of α-Chlorobenzenebutanenitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of α-Chlorobenzenebutanenitrile

Chemical Property:

Boiling Point:296.3±28.0 °C(Predicted)
Density:1.119±0.06 g/cm3(Predicted)

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of α-Chlorobenzenebutanenitrile

There total 4 articles about α-Chlorobenzenebutanenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 121054-03-3
2-hydroxy-4-phenylbutanenitrile

: 53279-93-9
rac-2-chloro-4-phenylbutanenitrile

Guidance literature:: With 1,3,5-trichloro-2,4,6-triazine; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; for 12h; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.orglett.7b03279

Reference yield:

: 104-53-0
3-phenyl-propionaldehyde

: 53279-93-9
rac-2-chloro-4-phenylbutanenitrile

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / diethyl ether / 20 °C / Inert atmosphere

2: hydrogenchloride / water / 2 h / 20 °C / Inert atmosphere

3: 1,3,5-trichloro-2,4,6-triazine / N,N-dimethyl-formamide; dichloromethane / 24 h / 20 °C / Inert atmosphere

With hydrogenchloride; 1,3,5-trichloro-2,4,6-triazine; potassium carbonate; In diethyl ether; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jacs.5b06466

Reference yield:

: 141377-52-8,134518-15-3
4-phenyl-2-(trimethylsilyloxy)butyronitrile

: 53279-93-9
rac-2-chloro-4-phenylbutanenitrile

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / water / 2 h / 20 °C / Inert atmosphere

2: 1,3,5-trichloro-2,4,6-triazine / N,N-dimethyl-formamide; dichloromethane / 24 h / 20 °C / Inert atmosphere

With hydrogenchloride; 1,3,5-trichloro-2,4,6-triazine; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jacs.5b06466