2H-IMidazo[4,5-c]pyridine-2-thione, 4-aMino-1,3-dihydro-1-[(4-Methoxyphenyl)Methyl]-

Base Information Edit

Chemical Name:2H-IMidazo[4,5-c]pyridine-2-thione, 4-aMino-1,3-dihydro-1-[(4-Methoxyphenyl)Methyl]-
CAS No.:1012059-50-5
Molecular Formula:C14H14N4OS
Molecular Weight:286.357
Hs Code.:2933990090
Mol file:1012059-50-5.mol

Synonyms:2H-IMidazo[4,5-c]pyridine-2-thione, 4-aMino-1,3-dihydro-1-[(4-Methoxyphenyl)Methyl]-

Suppliers and Price of 2H-IMidazo[4,5-c]pyridine-2-thione, 4-aMino-1,3-dihydro-1-[(4-Methoxyphenyl)Methyl]-

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
4-Amino-1-(4-methoxybenzyl)-1H-imidazo[4,5-c]pyridine-2(3H)-thione 95+%
1g
$ 772.00

Chemenu
4-amino-1-(4-methoxybenzyl)-1,3-dihydro-2H-imidazo[4,5-c]pyridine-2-thione 95%
1g
$ 729.00

American Custom Chemicals Corporation
4-AMINO-1-(4-METHOXYBENZYL)-1H-IMIDAZO[4,5-C]PYRIDINE-2(3H)-THIONE 95.00%
5MG
$ 496.53

Total 4 raw suppliers

Chemical Property of 2H-IMidazo[4,5-c]pyridine-2-thione, 4-aMino-1,3-dihydro-1-[(4-Methoxyphenyl)Methyl]- Edit

Chemical Property:

Boiling Point:492.5±55.0 °C(Predicted)
PKA:10.60±0.20(Predicted)
PSA：105.49000
Density:1.42±0.1 g/cm3(Predicted)
LogP:2.28920
Storage Temp.:2-8°C(protect from light)

Purity/Quality:

98%min ^*data from raw suppliers

4-Amino-1-(4-methoxybenzyl)-1H-imidazo[4,5-c]pyridine-2(3H)-thione 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2H-IMidazo[4,5-c]pyridine-2-thione, 4-aMino-1,3-dihydro-1-[(4-Methoxyphenyl)Methyl]-

There total 10 articles about 2H-IMidazo[4,5-c]pyridine-2-thione, 4-aMino-1,3-dihydro-1-[(4-Methoxyphenyl)Methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1012059-49-2
4-chloro-1-(4-methoxybenzyl)-1H-imidazo[4,5-c]pyridine-2(3H)-thione

: 1012059-50-5
4-amino-1-(4-methoxybenzyl)-1H-imidazo[4,5-c]pyridine-2(3H)-thione

Guidance literature:: 4-chloro-1-(4-methoxybenzyl)-1H-imidazo[4,5-c]pyridine-2(3H)-thione; With ammonia; sodium amide; at 20 ℃; for 30h;

With ethanol; at -40 ℃;

Reference yield: 75.0%

: 1012059-49-2
4-Chloro-1-(4-methoxybenzyl)-1H-imidazo[4,5-c]pyridine-2-thiol

: 1012059-50-5
4-amino-1-(4-methoxybenzyl)-1H-imidazo[4,5-c]pyridine-2-thiol

Guidance literature:: 4-Chloro-1-(4-methoxybenzyl)-1H-imidazo[4,5-c]pyridine-2-thiol; With sodium amide; In ammonia; at -78 - 20 ℃; Pressure bottle;

With acetic acid; In ethanol; water; pH=7;

Reference yield:

: 2393-23-9
4-methoxy-benzylamine

: 1012059-50-5
4-amino-1-(4-methoxybenzyl)-1H-imidazo[4,5-c]pyridine-2-thiol

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / N,N-dimethyl-formamide / 10 h / 0 - 20 °C

2.1: acetic acid; iron / 10 h / 40 °C

3.1: potassium hydroxide / ethanol; water / 12 h / Reflux

3.2: 20 °C / pH 7

4.1: sodium amide / ammonia / -78 - 20 °C / Pressure bottle

4.2: pH 7

With sodium amide; iron; acetic acid; triethylamine; potassium hydroxide; In ethanol; ammonia; water; N,N-dimethyl-formamide;