2-Hydroxy-2-azaadaMantane

Base Information

• Chemical Name: 2-Hydroxy-2-azaadaMantane
• CAS No.: 1155843-79-0
• Molecular Formula: C9H15NO
• Molecular Weight: 153.2215
• Mol file: 1155843-79-0.mol

Synonyms:2-Hydroxy-2-azaadaMantane

Chemical Property of 2-Hydroxy-2-azaadaMantane

Chemical Property:

• Boiling Point: 263.8±7.0 °C(Predicted)
• PKA: 13.91±0.20(Predicted)
• PSA: 23.47000
• Density: 1.201±0.06 g/cm3(Predicted)
• LogP: 1.57640

Purity/Quality:

98%,99%, ^*data from raw suppliers

2-Hydroxy-2-azaadamantane ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 2-Hydroxy-2-azaadamantane is a catalysis for the efficient C(sp3)-H bond functionalization of Isochroman.

Technology Process of 2-Hydroxy-2-azaadaMantane

There total 1 articles about 2-Hydroxy-2-azaadaMantane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(azaadamantane-N-oxyl)-1-trimethylsilyloxy-3-(3-butenyl)cyclohex-2-ene (1352617-22-1) → 2-azatricyclo[3.3.1.13,7]decan-2-ol (1155843-79-0) + 3-(3-butenyl)cyclohex-2-en-1-one (22627-45-8)

Guidance literature:

With hydrogenchloride; In dichloromethane; at 20 ℃; for 0.0833333h;

DOI:10.1021/ol2029417

Reference yield: 100.0%

2-azatricyclo[3.3.1.13,7]decan-2-ol (1155843-79-0) + C30H40B2FeN10O2 → C30H41B2FeN10O2

Guidance literature:

With oxygen; at -60 ℃; for 0.0833333h;

DOI:10.1002/anie.201502367

Reference yield: 92.0%

2-azatricyclo[3.3.1.13,7]decan-2-ol (1155843-79-0) → 2-azatricyclo[3.3.1.13,7 ]decane (768-41-2)

Guidance literature:

With hydrogen; In ethanol; water; at 25 ℃; for 4h; under 760.051 Torr;

DOI:10.1002/anie.201706594

upstream raw materials:

1-(azaadamantane-N-oxyl)-1-trimethylsilyloxy-3-(3-butenyl)cyclohex-2-ene

Downstream raw materials:

2-azatricyclo[3.3.1.13,7 ]decane

N-benzyl-2-azatricyclo[3.3.1.13,7]decane

2-azatricyclo[3.3.1.1^3,7]dec-2-yloxidanyl

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