N~5~,N~5~,1-trimethyl-1H-1,2,4-triazole-3,5-diamine(SALTDATA: FREE)

Base Information

• Chemical Name: N~5~,N~5~,1-trimethyl-1H-1,2,4-triazole-3,5-diamine(SALTDATA: FREE)
• CAS No.: 26668-70-2
• Molecular Formula: C5H11N5
• Molecular Weight: 141.17
• Hs Code.: 2933990090
• Mol file: 26668-70-2.mol

Synonyms:N~5~,N~5~,1-trimethyl-1H-1,2,4-triazole-3,5-diamine(SALTDATA: FREE)

Chemical Property of N~5~,N~5~,1-trimethyl-1H-1,2,4-triazole-3,5-diamine(SALTDATA: FREE)

Chemical Property:

• Melting Point: 136.5 °C
• Boiling Point: 303.5±25.0 °C(Predicted)
• PKA: 5.89±0.10(Predicted)
• PSA: 60.70000
• Density: 1.28±0.1 g/cm3(Predicted)
• LogP: -0.60660

Purity/Quality:

98% ^*data from raw suppliers

N5,N5,1-trimethyl-1H-1,2,4-triazole-3,5-diamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N~5~,N~5~,1-trimethyl-1H-1,2,4-triazole-3,5-diamine(SALTDATA: FREE)

There total 3 articles about N~5~,N~5~,1-trimethyl-1H-1,2,4-triazole-3,5-diamine(SALTDATA: FREE) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

methylhydrazine (60-34-4) + N'-cyano-N,N-dimethyl-S-methylisothiourea → 3-Amino-5-(dimethylamino)-1-methyl-1H-1,2,4-triazol (26668-70-2) + 5-Amino-3-(dimethylamino)-1-methyl-1H-1,2,4-triazol (87009-70-9)

Guidance literature:

In N,N-dimethyl-formamide; Ambient temperature;

DOI:10.1002/hlca.19830660416

Reference yield:

dimethyl-(2-methyl-5-nitro-2H-[1,2,4]triazol-3-yl)-amine (26668-66-6) → 3-Amino-5-(dimethylamino)-1-methyl-1H-1,2,4-triazol (26668-70-2)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol;

Reference yield:

→ 3-Amino-5-(dimethylamino)-1-methyl-1H-1,2,4-triazol (26668-70-2)

Guidance literature:

Triazol IId, H2/Pd-C;

DOI:10.1007/BF00475007

upstream raw materials:

methylhydrazine

dimethyl-(2-methyl-5-nitro-2H-[1,2,4]triazol-3-yl)-amine

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