2-(naphthalen-2-yl)phenylboronic acid

Base Information

Chemical Name:2-(naphthalen-2-yl)phenylboronic acid
CAS No.:1061350-97-7
Molecular Formula:C16H13BO2
Molecular Weight:248.089
Hs Code.:2931900090
Mol file:1061350-97-7.mol

Synonyms:2-(naphthalen-2-yl)phenylboronic acid;B-[2-(2-Naphthalenyl)phenyl]boronic acid

Suppliers and Price of 2-(naphthalen-2-yl)phenylboronic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
(2-(Naphthalen-2-yl)phenyl)boronicacid 97%
5g
$ 302.00

Crysdot
(2-(Naphthalen-2-yl)phenyl)boronicacid 97%
1g
$ 79.00

Chemenu
(2-(Naphthalen-2-yl)phenyl)boronicacid 97%
1g
$ 62.00

Chemenu
(2-(Naphthalen-2-yl)phenyl)boronicacid 97%
5g
$ 242.00

American Custom Chemicals Corporation
2-(NAPHTHALENE-2-YL)PHENYLBORONIC ACID 95.00%
1G
$ 205.91

Alichem
2-(Naphthalen-2-yl)phenylboronicacid
1g
$ 1617.60

Alichem
2-(Naphthalen-2-yl)phenylboronicacid
500mg
$ 1029.00

Alichem
2-(Naphthalen-2-yl)phenylboronicacid
250mg
$ 700.40

Total 24 raw suppliers

Chemical Property of 2-(naphthalen-2-yl)phenylboronic acid

Chemical Property:

Boiling Point:479.7±48.0 °C(Predicted)
PKA:8.50±0.58(Predicted)
PSA：40.46000
Density:1.23
LogP:2.18660
Storage Temp.:2-8°C

Purity/Quality:

97% ^*data from raw suppliers

(2-(Naphthalen-2-yl)phenyl)boronicacid 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-(naphthalen-2-yl)phenylboronic acid

There total 5 articles about 2-(naphthalen-2-yl)phenylboronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.1%

: 121-43-7,63156-11-6
Trimethyl borate

: 22082-97-9
1-bromo-2-(2-naphthyl)benzene

: 7732-18-5
water

: 1061350-97-7
2-(naphthalen-2-yl)phenylboronic acid

Guidance literature:: 1-bromo-2-(2-naphthyl)benzene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 1h;

Trimethyl borate; In tetrahydrofuran; hexane; at 20 ℃; for 12h;

water; With hydrogenchloride; In tetrahydrofuran; hexane; for 5h;

Reference yield: 60.0%

: 121-43-7,63156-11-6
Trimethyl borate

: 22082-97-9
1-bromo-2-(2-naphthyl)benzene

: 1061350-97-7
2-(naphthalen-2-yl)phenylboronic acid

Guidance literature:: 1-bromo-2-(2-naphthyl)benzene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

Trimethyl borate; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 1h;
DOI:10.1055/s-0035-1561940

Reference yield:

: 32316-92-0
naphthalene-2-boronic acid

: 1061350-97-7
2-(naphthalen-2-yl)phenylboronic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / toluene / 4 h / Inert atmosphere; Reflux

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 - 20 °C

2.2: 12 h / 20 °C

2.3: 5 h

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; potassium carbonate; In tetrahydrofuran; hexane; toluene;