1,5,5-Trimethyl-6-(1,3-butadiene-1-yl)-1-cyclohexene

Base Information

• Chemical Name: 1,5,5-Trimethyl-6-(1,3-butadiene-1-yl)-1-cyclohexene
• CAS No.: 56248-15-8
• Molecular Formula: C₁₃H₂₀
• Molecular Weight: 176.302
• Mol file: 56248-15-8.mol

Synonyms:1,5,5-Trimethyl-6-(1,3-butadiene-1-yl)-1-cyclohexene;6-(1,3-Butadienyl)-1,5,5-trimethyl-1-cyclohexene

Chemical Property of 1,5,5-Trimethyl-6-(1,3-butadiene-1-yl)-1-cyclohexene

Chemical Property:

• Boiling Point: 96-97 °C(Press: 16.5 Torr)
• Density: 0.8675 g/cm3(Temp: 18 °C)

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,5,5-Trimethyl-6-(1,3-butadiene-1-yl)-1-cyclohexene

There total 5 articles about 1,5,5-Trimethyl-6-(1,3-butadiene-1-yl)-1-cyclohexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

alpha-ionol (25312-34-9) → (1'E)-6-(buta-1',3'-dienyl)-1,5,5-trimethylcyclohex-1-ene (51768-73-1,56248-15-8) + (1'Z)-6-(buta-1',3'-dienyl)-1,5,5-trimethylcyclohex-1-ene (85329-76-6,56248-15-8)

Guidance literature:

With N,N,N,N,N,N-hexamethylphosphoric triamide; at 215 - 230 ℃; for 0.5h; Yield given. Yields of byproduct given;

Reference yield:

alpha-ionol (25312-34-9) → (1'E)-6-(buta-1',3'-dienyl)-1,5,5-trimethylcyclohex-1-ene (51768-73-1,56248-15-8) + (1'Z)-6-(buta-1',3'-dienyl)-1,5,5-trimethylcyclohex-1-ene (85329-76-6,56248-15-8)

Guidance literature:

With N,N,N,N,N,N-hexamethylphosphoric triamide; at 215 - 230 ℃; for 0.5h; Yield given. Yields of byproduct given;

Reference yield:

beta-Ionol (472-80-0,35031-11-9,53078-25-4,53108-96-6,81600-95-5,81801-17-4,83348-85-0,22029-76-1,27008-60-2) + α-ionol (472-78-6) → 6-(2-butenylidene)-1,5,5-trimethylcyclohexene (55497-53-5) + megastigma-4,7,9-triene (56248-15-8) + megastigma-5,7,9-triene

Guidance literature:

In carbon dioxide; isopropyl alcohol; at 230 ℃; Concentration; Temperature; liquid CO₂;

DOI:10.1134/S0036024413110046

upstream raw materials:

alpha-ionol

beta-Ionol

α-ionol

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