tert-Butyl 2-(2-methyl-1-nitropropan-2-yl)hydrazinecarboxylate

Base Information

• Chemical Name: tert-Butyl 2-(2-methyl-1-nitropropan-2-yl)hydrazinecarboxylate
• CAS No.: 1354825-84-5
• Molecular Formula: C₉H₁₉N₃O₄
• Molecular Weight: 233.268
• Hs Code.: 2928009090
• Mol file: 1354825-84-5.mol

Synonyms:tert-Butyl 2-(2-methyl-1-nitropropan-2-yl)hydrazinecarboxylate

Chemical Property of tert-Butyl 2-(2-methyl-1-nitropropan-2-yl)hydrazinecarboxylate

Chemical Property:

• PKA: 12.09±0.43(Predicted)
• PSA: 96.18000
• Density: 1.105±0.06 g/cm3(Predicted)
• LogP: 2.37600

Purity/Quality:

97% ^*data from raw suppliers

tert-Butyl2-(2-Methyl-1-nitropropan-2-yl)hydrazinecarboxylate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of tert-Butyl 2-(2-methyl-1-nitropropan-2-yl)hydrazinecarboxylate

There total 1 articles about tert-Butyl 2-(2-methyl-1-nitropropan-2-yl)hydrazinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

1-Nitro-2-methyl-1-propen (1606-30-0) + t-butoxycarbonylhydrazine (870-46-2) → N'-(1,1-dimethyl-2-nitro-ethyl)-hydrazinecarboxylic acid tert-butyl ester (1354825-84-5)

Guidance literature:

In water; acetonitrile; for 1h;

Reference yield:

N'-(1,1-dimethyl-2-nitro-ethyl)-hydrazinecarboxylic acid tert-butyl ester (1354825-84-5) → N'-(2-benzyloxycarbonylamino-1,1-dimethyl-ethyl)hydrazinecarboxylic acid tert-butyl ester (1354825-85-6)

Guidance literature:

Multi-step reaction with 2 steps

1: ammonium formate / palladium 10% on activated carbon / methanol / 1 h / 20 °C

2: triethylamine / acetonitrile / 16 h / 20 °C

With ammonium formate; triethylamine; palladium 10% on activated carbon; In methanol; acetonitrile;

upstream raw materials:

1-Nitro-2-methyl-1-propen

t-butoxycarbonylhydrazine

Downstream raw materials:

N'-(2-benzyloxycarbonylamino-1,1-dimethyl-ethyl)hydrazinecarboxylic acid tert-butyl ester

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